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Focused on in-situ utilization of lunar resources, we studied the preparation of aluminum alloy by aluminothermic reduction of ilmenite in molten cryolite media. The standard Gibbs free energy change of aluminothermic reduction of ilmenite are negative at temperature range 0-1500℃. The effects of reductant amount and reaction time on the aluminothermic reduction of ilmenite in 47.14mass%NaF-42.86mass%AlF₃-10mass%?TiO₃ at 960℃ were studied. The results obtained by XRF, XRD, SEM and EDS analysis show that the products mainly contain Al, Ti, Fe, and little Si, and the main phase of the product is Al₃Ti. With the increase of reductant amount, the content of Ti in alloy products decreases, while the content of Fe in alloy products increases. In addition, the content of Al₃Ti increases with the increase of reaction time. The highest content of Ti in the alloy obtained by aluminothermic reaction for 2h at 960℃ using three times reductant amount of theoretical amount is up to 18.82 mass%. Fe and Ti can be separated when FeTiO₃ aluminothermic reduction was carried using lower reductant amount and higher reduction time. The FeTiO₃ aluminothermic reduction reaction takes place between the dissolved Al atom and dissolved FeTiO₃ in the Cryolite melt.