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鎢表面形貌控制及其在循環(huán)熱載荷作用下的熱疲勞性能
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北京工業(yè)大學(xué) 材料科學(xué)與工程學(xué)院,北京工業(yè)大學(xué) 材料科學(xué)與工程學(xué)院,北京工業(yè)大學(xué) 材料科學(xué)與工程學(xué)院,北京工業(yè)大學(xué) 材料科學(xué)與工程學(xué)院,北京工業(yè)大學(xué) 材料科學(xué)與工程學(xué)院,北京工業(yè)大學(xué) 材料科學(xué)與工程學(xué)院

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Surface morphology controlled of tungsten and its thermal fatigue behavior under cyclic heat loading
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School of Materials Science and Engineering,Beijing University of Technology,School of Materials Science and Engineering,Beijing University of Technology,School of Materials Science and Engineering,Beijing University of Technology,School of Materials Science and Engineering,Beijing University of Technology,School of Materials Science and Engineering,Beijing University of Technology,School of Materials Science and Engineering,Beijing University of Technology

Fund Project:

National Magnetic Confinement Fusion Science Program of China (2013GB109003); National Nature Science Foundation of China (51571003)

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    摘要:

    鎢作為聚變裝置中的壁材料在各種循環(huán)熱載荷作用下的熱疲勞行為是一個重要的問題,它的熱疲勞行為可能會受到其表面形貌的影響。為了解決這個問題,采用電子回旋共振(ECR)等離子體系統(tǒng)在多晶鎢表面進(jìn)行形貌控制實驗,然后采用電子束設(shè)備對拋光和具有一定形貌的樣品開展循環(huán)熱載荷實驗。結(jié)果表明表面形貌對在循環(huán)載荷下發(fā)生的循環(huán)塑性變形造成的損傷特征影響很小,在300次循環(huán)熱載荷下某些晶粒中形成了微裂紋及擠出片結(jié)構(gòu),它們在不同晶粒中按著某一特定的方向平行排列。此外,在不同條件下通過等離子體刻蝕在鎢表面制備了不同的三棱錐狀和均勻的納米結(jié)構(gòu)。本文中,我們對損傷區(qū)域的截面進(jìn)行了分析并給出了在循環(huán)熱載荷下這種結(jié)構(gòu)形成過程的示意圖。

    Abstract:

    Thermal fatigue behavior under various cyclic heat loading is an important concern for tungsten as armor material in fusion devices. It may be significantly affected by its surface morphology. To address this issue, surface morphology controlled experiments have been performed on polycrystalline tungsten using an ECR plasma system and cyclic heat loading tests have been conducted upon the polished and modified samples using an electron beam facility. The results indicate that the surface topography has little effect on the characteristics of damage caused by the cycle plastic deformation during the cyclic heat loading. The micro-cracks and extrusions are formed in some grains after suffered 300 cyclic heat loading, which are aligned in different directions for varying grains. In addition, the modified specimens have fabricated both different triangular pyramid and homogeneous nanostructures by dry etching with different conditions. In this work, the cross-sectional surface of damage regions were analyzed and a set of schematic diagram was presented to explain the mechanism for the formation of micro-cracks and extrusions under cyclic heat loading.

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王亮,王波,李曙丹,湯云暉,宋雪梅,嚴(yán)輝.鎢表面形貌控制及其在循環(huán)熱載荷作用下的熱疲勞性能[J].稀有金屬材料與工程,2018,47(6):1729~1733.[Wang Liang, Wang Bo, Li Shudan, Tang Yunhui, Song Xuemei, Yan Hui. Surface morphology controlled of tungsten and its thermal fatigue behavior under cyclic heat loading[J]. Rare Metal Materials and Engineering,2018,47(6):1729~1733.]
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  • 收稿日期:2016-04-18
  • 最后修改日期:2016-07-14
  • 錄用日期:2016-08-17
  • 在線發(fā)布日期: 2018-09-06
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