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溫度對真空熱壓連接技術制備AZ31/Al/Ta復合材料界面組織和力學性能的影響
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華北電力大學 先進材料研究院

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Effect of Temperature on the Interface Microstructure andMechanical Properties of AZ31/Al/Ta Composites Prepared by Vacuum Hot Compression Bonding
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Affiliation:

1.Institute for Advanced Materials,North China Electric Power University;2.Beijing Institute of Spacecraft System Engineering

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National Natural Science Foundation of China (No.52275308; No.52301146), The Fundamental Research Funds for the Central Universities (2023JG007), and funding from Shi Changxu Innovation Center for Advanced Materials (SCXKFJJ202207).

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    摘要:

    Mg/Ta 復合材料兼具抗高能粒子輻照和輕質特性,這使其能夠更好的滿足未來深空探測需求。然而,由于這兩種不同金屬在性能上存在顯著差異,將它們連接起來頗具挑戰(zhàn)性。本文采用真空熱壓連接方法成功制備了AZ31/Al/Ta復合材料。研究了熱壓溫度對AZ31/Al/Ta復合材料界面組織演變、相組成及界面剪切強度的影響。探討了AZ31/Al/Ta復合材料在VHCB工藝條件下的界面結合機理。結果表明,隨著熱壓溫度的升高,Mg-Al界面相組成由Mg-Al脆性IMC(Al12Mg17,Al3Mg2)轉變?yōu)锳l-Mg固溶體。與400℃相比,450℃時Al/Ta界面擴散層寬度增大。在400℃和450℃時,AZ31/Al/Ta復合材料抗剪強度分別為24 MPa和46 MPa。AZ31/Al/Ta復合材料界面結合機制為擴散與機械嚙合共存。此外,避免界面脆性相的形成可以顯著提高界面結合強度。

    Abstract:

    The Mg/Ta composite material exhibits both exceptional resistance to high-energy particle irradiation and lightweight characteristics, enabling it to more effectively address the requirements of future deep-space exploration. However, joining these two dissimilar metals is challenging due to their significant differences in properties. In this work, AZ31/Al/Ta composites were successfully prepared using the vacuum hot compression bonding (VHCB) method. The effect of hot compressing temperature on the interface microstructure evolution, phase constitution, and shear strength at the interface was investigated. Moreover, the interface bonding mechanisms of the AZ31/Al/Ta composites under the VHCB process conditions were explored. The results demonstrated that as the VHCB temperature increased, the phase composition of the interface between Mg and Al changed from the Mg-Al brittle IMCs (Al12Mg17, Al3Mg2) to the Al-Mg solid solution. Meanwhile, the width of the Al/Ta interface diffusion layer increased to 450℃ compared to that at 400℃. The shear strengths were 24 MPa and 46 MPa at 400℃ and 450℃, respectively. The interfacial bonding mechanism of AZ31/Al/Ta composites involves the coexistence of diffusion and mechanical meshing. Avoiding the formation of brittle phases at the interface can significantly improve interfacial bonding strength.

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于智磊,李景利,韓修柱,李佰銳,薛志勇.溫度對真空熱壓連接技術制備AZ31/Al/Ta復合材料界面組織和力學性能的影響[J].稀有金屬材料與工程,,().[Yu Zhilei, Li Jingli, Han Xiuzhu, Li Bairui, Xue Zhiyong. Effect of Temperature on the Interface Microstructure andMechanical Properties of AZ31/Al/Ta Composites Prepared by Vacuum Hot Compression Bonding[J]. Rare Metal Materials and Engineering,,().]
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  • 收稿日期:2024-09-17
  • 最后修改日期:2024-11-18
  • 錄用日期:2024-12-02
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