-1。建立了U720Li合金在這2種保溫時(shí)間下的熱加工圖。通過分析熱加工圖各區(qū)域?qū)?yīng)的變形組織,明確了保溫5 min的最佳熱加工條件為1090~1110 ℃/1~10 s-1和1146~1180 ℃/1~10 s-1,而保溫10 min的最佳熱加工條件為1080~1090 ℃/1~10 s-1和1153~1160 ℃/ 1~10 s-1。可見適當(dāng)縮短變形前保溫時(shí)間可擴(kuò)大該合金的安全加工窗口。在未發(fā)生開裂的情況下,動(dòng)態(tài)再結(jié)晶(DRX)晶粒隨變形溫度和保溫時(shí)間的增加而逐漸增大,但隨應(yīng)變速率的增加先減小后增大。當(dāng)變形溫度低于1100 ℃,主要DRX機(jī)制為顆粒誘導(dǎo)連續(xù)DRX。當(dāng)變形溫度高于1130 ℃,主要DRX機(jī)制轉(zhuǎn)變?yōu)椴贿B續(xù)DRX。"/>

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保溫時(shí)間對(duì)難變形高溫合金U720Li熱變形行為的影響
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作者單位:

1.沈陽工業(yè)大學(xué) 材料科學(xué)與工程學(xué)院,遼寧 沈陽 110870;2.遼寧科技大學(xué) 材料與冶金學(xué)院,遼寧 鞍山 114051;3.中國(guó)科學(xué)院 金屬研究所,遼寧 沈陽 110016

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基金項(xiàng)目:

國(guó)家自然科學(xué)基金項(xiàng)目(面上項(xiàng)目,重點(diǎn)項(xiàng)目,重大項(xiàng)目)(52174317、51904146)


Influence of Holding Time on Hot Deformation Behavior of Hard-Deformed Superalloy U720Li
Author:
Affiliation:

1.School of Materials Science and Engineering, Shenyang University of Technology, Shenyang 110870, China;2.School of Materials and Metallurgy, University of Science and Technology Liaoning, Anshan 114051, China;3.Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China

Fund Project:

National Natural Science Foundation of China (52174317, 51904146)

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    摘要:

    為了改善難變形高溫合金U720Li的熱加工性能,研究了變形前保溫時(shí)間(5和10 min)對(duì)該合金的熱變形行為的影響。結(jié)果表明,流動(dòng)應(yīng)力隨應(yīng)變速率的提高而增大,但隨變形溫度和保溫時(shí)間的增加而減小。依據(jù)所建立的Arrhenius本構(gòu)模型計(jì)算的峰值應(yīng)力與實(shí)驗(yàn)值吻合良好,說明該模型可準(zhǔn)確預(yù)測(cè)U720Li合金熱變形行為。保溫時(shí)間為5和10 min的熱變形激活能分別為992.006和850.996 kJ·mol-1。建立了U720Li合金在這2種保溫時(shí)間下的熱加工圖。通過分析熱加工圖各區(qū)域?qū)?yīng)的變形組織,明確了保溫5 min的最佳熱加工條件為1090~1110 ℃/1~10 s-1和1146~1180 ℃/1~10 s-1,而保溫10 min的最佳熱加工條件為1080~1090 ℃/1~10 s-1和1153~1160 ℃/ 1~10 s-1??梢娺m當(dāng)縮短變形前保溫時(shí)間可擴(kuò)大該合金的安全加工窗口。在未發(fā)生開裂的情況下,動(dòng)態(tài)再結(jié)晶(DRX)晶粒隨變形溫度和保溫時(shí)間的增加而逐漸增大,但隨應(yīng)變速率的增加先減小后增大。當(dāng)變形溫度低于1100 ℃,主要DRX機(jī)制為顆粒誘導(dǎo)連續(xù)DRX。當(dāng)變形溫度高于1130 ℃,主要DRX機(jī)制轉(zhuǎn)變?yōu)椴贿B續(xù)DRX。

    Abstract:

    To improve the hot workability of hard-deformed superalloy U720Li, the effect of holding time before deformation (5 and 10 min) on hot deformation behavior was investigated by hot compression tests. Results show that the flow stress increases with increase in strain rate, while decreases with increase in deformation temperature and holding time. Based on the obtained Arrhenius-type constitutive models, the calculated peak stresses are in good agreement with experimental values, indicating that this model can accurately predict the hot deformation behavior of U720Li alloy, and the deformation activation energies for the holding time of 5 and 10 min were calculated to be 992.006 and 850.996 kJ·mol-1, respectively. Moreover, processing maps of U720Li alloy with these two holding durations were constructed. Through observation of deformation microstructures in each domain of the processing maps, the optimal hot working conditions for the holding time of 5 min are determined to be 1090?1110 °C/ 1?10 s-1 and 1146?1180 °C/1?10 s-1, and the optimal hot working conditions for the holding time of 10 min are 1080?1090 °C/1?10 s-1 and 1153?1160 °C/1?10 s-1, indicating that the safe processing window can be obviously enlarged by shortening the holding time reasonably. In the absence of cracking, the dynamic recrystallization (DRX) grain size increases gradually with increasing the deformation temperature and holding time, but it first decreases and then increases with the increase in strain rate. When the deformation temperature is below 1100 °C, the DRX mechanism is mainly the particle-induced continuous DRX. As the temperature is raised to above 1130 °C, the main DRX mechanism changes to discontinuous DRX.

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臧喜民,趙廣迪,武金江,姜昊源,姚曉雨.保溫時(shí)間對(duì)難變形高溫合金U720Li熱變形行為的影響[J].稀有金屬材料與工程,2024,53(9):2446~2457.[Zang Ximin, Zhao Guangdi, Wu Jinjiang, Jiang Haoyuan, Yao Xiaoyu. Influence of Holding Time on Hot Deformation Behavior of Hard-Deformed Superalloy U720Li[J]. Rare Metal Materials and Engineering,2024,53(9):2446~2457.]
DOI:10.12442/j. issn.1002-185X.20230790

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  • 收稿日期:2023-12-05
  • 最后修改日期:2024-01-24
  • 錄用日期:2024-02-01
  • 在線發(fā)布日期: 2024-09-12
  • 出版日期: 2024-09-04