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預(yù)變形Mo-0.3La合金的熱變形行為研究
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1.西安建筑科技大學(xué) 冶金學(xué)院;2.金堆城鉬業(yè)股份有限公司

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陜西省科技重大專項(xiàng)資助(項(xiàng)目號(hào)2020zdzx04-02-01),陜西省青年科技新星項(xiàng)目資助(項(xiàng)目號(hào)2019KJXX-005)


The Study on hot deformation behavior of Pre-Deformation Mo-0.3La AlloyZhang Xiao1,3,4,Wang Kuaishe1,2,Feng Pengfa3,4,An geng3,4,Bu chunyang3,4,Hu Ping1,2,Xi Sha3,4,Li Jing3,4,Zhou Sha3,4
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陜西省科技重大專項(xiàng)資助(項(xiàng)目號(hào)2020zdzx04-02-01),陜西省青年科技新星項(xiàng)目資助(項(xiàng)目號(hào)2019KJXX-005)

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    摘要:

    采用Gleeble-3500熱模擬機(jī)在變形溫度為700~1273K、應(yīng)變速率為0.001~0.1 s-1、真應(yīng)變?yōu)?0%的實(shí)驗(yàn)條件下,對(duì)預(yù)變形Mo-0.3La合金的熱變形行為進(jìn)行了研究,并采用包含Zene-Hollomon參數(shù)的雙曲正弦模型,建立了熱變形流變方程。結(jié)果表明:預(yù)變形Mo-0.3La合金的真應(yīng)力-應(yīng)變曲線具有動(dòng)態(tài)再結(jié)晶特征,在較低的溫度(973K)/較高的應(yīng)變速率(0.1 s-1)下,表現(xiàn)出加工硬化,在1273K低應(yīng)變速率(0.001和0.005 s-1)下動(dòng)態(tài)再結(jié)晶具有顯著性;合金含有31.65%大角度晶界,再變形后大角度晶界減少至17.14%,且存在少量的再結(jié)晶晶粒(6.08%);變形溫度升高,大角度晶界和再結(jié)晶晶粒增多;由流變方程得到平均變形激活能Q為287.08kJ/mol,應(yīng)力指數(shù)n為14.40,依據(jù)流變方程計(jì)算出的應(yīng)力理論值與實(shí)際值的平均相對(duì)誤差僅3.25%。

    Abstract:

    The hot deformation behavior of pre-deformation Mo-0.3La alloy was studied on the Gleeble-3500 thermal-mechanical simulator at 973~1273K with the rate of deformation 0.001~0.1 s-1 and the true strain of 60%, and the constitutive equation was established by hyperbolic sine model with Zene-Hollomon parameter. The results show that in this experimental conditions, the dynamic recrystallization characteristics of the true stress-strain curves are observed. Pre-deformation Mo-0.3La alloy, at high strain rate 0.1 s?1 or low temperature 973K exhibits workhardening, dynamic recrystallization is significant at low strain rates (0.001 and 0.005s-1) of 1273K. The high angle grain boundaries of the pre-deformation alloy is 31.65%. After redeformation, the high grain boundary decreases to 17.14%, and there are a small amount of recrystallized grains(6.08%), with the increase of deformation temperature, high grain boundaries and recrystallized grains increase. Calculated by the constitutive equation, the deformation activation energy Q is 287.08 kJ/mol, and the stress exponent n is 14.40. Using this equation, the average relative error between the theoretical calculations and experimental results is only 3.25%.

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引用本文

張曉,王快社,馮鵬發(fā),安耿,卜春陽,胡平,席莎,李晶,周莎.預(yù)變形Mo-0.3La合金的熱變形行為研究[J].稀有金屬材料與工程,2024,53(12):3390~3397.[Zhang Xiao, Wang Kuaishe, Feng Pengfa, An geng, Bu Chunyang, Hu Ping, Xi Sha, Li Jing, Zhou Sha. The Study on hot deformation behavior of Pre-Deformation Mo-0.3La AlloyZhang Xiao1,3,4,Wang Kuaishe1,2,Feng Pengfa3,4,An geng3,4,Bu chunyang3,4,Hu Ping1,2,Xi Sha3,4,Li Jing3,4,Zhou Sha3,4[J]. Rare Metal Materials and Engineering,2024,53(12):3390~3397.]
DOI:10.12442/j. issn.1002-185X.20230773

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  • 收稿日期:2023-11-30
  • 最后修改日期:2024-01-23
  • 錄用日期:2024-01-31
  • 在線發(fā)布日期: 2024-12-23
  • 出版日期: 2024-12-16