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固溶處理工藝對一種鎳基單晶高溫合金長期時效后持久性能的影響
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1.中國科學院金屬研究所師昌緒先進材料創(chuàng)新中心高溫結構材料研究部;2.東北大學軋制技術及連軋自動化國家重點實驗室

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Effect of solution treatment on creep rupture properties after long-term aging of a Nickel-based single crystal superalloy
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1.Shi-Changxu Innovation Center for Advanced Materials,Institute of Metal Research,Chinese Academy of Sciences;2.The State Key Laboratory of Rolling and Automation,Northeastern University

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    摘要:

    本文通過對一種傳統(tǒng)鎳基單晶高溫合金在不同熱處理工藝條件下的固溶和時效進行實驗,研究了固溶時間和長期時效對合金微觀組織和性能的影響。結果表明:鎳基單晶高溫合金較佳的熱處理工藝為1310℃/4h(空冷)+1130℃/4h(空冷)+899℃/16h(空冷)。經過固溶處理后,極大程度避免析出不利TCP相,獲得尺寸較小、立方度較高的強化相γ′的微觀組織。不同熱處理制度下,合金持久斷裂壽命和延展率相差較小。變形過程中,脆性針狀TCP相優(yōu)先破碎,不是裂紋萌生處。而枝晶間的薄弱的碳化物/基體界面提供了裂紋的源頭。

    Abstract:

    In this research, the effects of solution time and long-term aging on microstructure evolution and mechanical properties of a traditional nickel-based single crystal superalloy under different heat treatment conditions were studied. The obtained results demonstrate that the best heat treatment regime is “1310℃/4h (AC)+1130℃/4h (AC)+899℃/16h (AC)”. After the solution treatment, the participating of adverse phase of TCP has been avoided to obtain the preferable microstructure with small size and a high degree of cubic of strengtheningγ′phase. The difference in creep rupture life and percentage of elongation is slight under different heat treatment regimes. During the deformation, the brittle TCP phase was broken first, demonstrating that it is not the crack initiation. However, the weak carbide/matrix interface in inter-dendrites is the source of the crack.

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王楠,劉紀德,朱崇偉,張志鵬,徐偉,李金國.固溶處理工藝對一種鎳基單晶高溫合金長期時效后持久性能的影響[J].稀有金屬材料與工程,2024,53(11):3129~3135.[Nan Wang, Jide Liu, Congwei Zhu, Zhipeng Zhang, Wei Xu, Jinguo Li. Effect of solution treatment on creep rupture properties after long-term aging of a Nickel-based single crystal superalloy[J]. Rare Metal Materials and Engineering,2024,53(11):3129~3135.]
DOI:10.12442/j. issn.1002-185X.20230532

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歷史
  • 收稿日期:2023-08-30
  • 最后修改日期:2024-01-04
  • 錄用日期:2024-01-05
  • 在線發(fā)布日期: 2024-11-20
  • 出版日期: 2024-11-08