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預(yù)熱處理對(duì)一種新型鎳基粉末高溫合金渦輪盤鍛態(tài)顯微組織的影響
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1.中南大學(xué) 粉末冶金國家重點(diǎn)實(shí)驗(yàn)室;2.深圳市萬澤中南研究院有限公司

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廣東省引進(jìn)創(chuàng)新創(chuàng)業(yè)團(tuán)隊(duì)項(xiàng)目資助 607264877417,國家科技重大專項(xiàng)( 2017-Ⅵ-0009-0080 ),深圳市工業(yè)和信息化局項(xiàng)目(201806071114243770)


Miscrostructure study of preheating treatment on a Novel Nickel-Based Superalloy turbine disc
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Supported by Guangdong Innovative and Entrepreneurial Research Team Program 607264877417,National Science and Technology Major Project(2017-Ⅵ-0009-0080),Industry and Information Technology Bureau of Shenzhen Municipality (Project No. 201806071114243770)

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    摘要:

    本工作研究了復(fù)合亞固溶熱處理工藝對(duì)一種新型鎳基粉末高溫合金FGH4113A(WZ-A3)γ"相組織的影響規(guī)律。大尺寸鍛造態(tài)渦輪盤件鍛后冷速較低,γ"相的尺寸在約100nm至4500nm之間分布。在盤件上取小試樣進(jìn)行熱處理實(shí)驗(yàn),試樣升溫至1000℃和1050℃時(shí),γ"相總占比下降,Oswald熟化機(jī)制及PAM機(jī)制同時(shí)存在。試樣升溫至1100℃時(shí),晶內(nèi)γ"相完全回溶。使用復(fù)合亞固溶熱處理工藝,先將試樣升溫至1120℃度保溫2h,快速冷卻后再分別升溫至1000℃、1050℃和1100℃時(shí),γ"相總占比均下降,晶內(nèi)γ"相演變以O(shè)swald熟化機(jī)制為主導(dǎo),其形貌及尺寸在升溫過程中相對(duì)穩(wěn)定。在盤件上取性能試棒分別進(jìn)行鍛造態(tài)+1000℃(不保溫)+時(shí)效熱處理和鍛造態(tài)+1120℃(2h),80℃/min+1000℃空冷+時(shí)效熱處理后進(jìn)行550℃拉伸測(cè)試,后者的屈服強(qiáng)度和抗拉強(qiáng)度顯著高于前者,可為大尺寸渦輪盤件的雙性能熱處理工藝的制定提供參考。

    Abstract:

    The effect of two-step sub-solvus heat treatment process on the γ "phase microstructure of a novel nickel-based powder metallurgy superalloy FGH4113A (WZ-A3) was studied. The cooling rate of large-size forged turbine disc is lower after forging, and the size distribution of γ" phases is from about 100nm to 4500nm. Small samples were taken from the disc for heat treatment experiments. When the samples were heated to 1000 ℃ and 1050 ℃, the total proportion of γ "phases decreased, and the evolution mechanism showed signs of Oswald coarsening mechanism and PAM mechanism. When the sample was heated to 1100 ℃, the intracrystalline γ" phase was completely dissolved. If two-step sub-solid solution heat treatment process was used, the sample was first heated to 1120 ℃ for 2h followed by rapid cooling, and then heated to 1000 ℃, 1050 ℃ or 1100 ℃, the total proportion of γ "phases decreased. The evolution of intracrystalline γ" phases was dominated by the Oswald coarsening mechanism, and its morphology and size were relatively stable during the heating process. The testing rods were cut from the disc and went through as forged state + 1000 ℃ (without heat preservation) + aging heat treatment and as forged state + 1120 ℃ (2h) + aging heat treatment respectively, and followed by tensile test at 550 ℃. The yield and tensile strengths of the latter one are significantly higher than the first one, and this can be treated as a reference for dual-performance heat treatment process design of large-size turbine discs.

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劉朝峰,程俊義,馬向東,肖磊,郭建政,馮干江.預(yù)熱處理對(duì)一種新型鎳基粉末高溫合金渦輪盤鍛態(tài)顯微組織的影響[J].稀有金屬材料與工程,2024,53(3):768~777.[liuzhaofeng, chengjunyi, maxiangdong, xiaolei, guojianzheng, fengganjiang. Miscrostructure study of preheating treatment on a Novel Nickel-Based Superalloy turbine disc[J]. Rare Metal Materials and Engineering,2024,53(3):768~777.]
DOI:10.12442/j. issn.1002-185X.20230519

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  • 收稿日期:2023-08-22
  • 最后修改日期:2023-11-13
  • 錄用日期:2023-11-17
  • 在線發(fā)布日期: 2024-03-27
  • 出版日期: 2024-03-20