-1時的熱變形行為。根據(jù)壓縮數(shù)據(jù)獲得真應力-真應變曲線,分析了變形溫度和應變速率對電解鎳力學性能的影響,并得到流變應力本構方程,基于動態(tài)材料模型及Prassd失穩(wěn)準則建立了熱加工圖。結果表明:電解鎳對變形溫度和應變速率表現(xiàn)出較強的敏感性,隨變形溫度的升高和應變速率的降低,流變應力逐漸減小;隨應變的增加,流變應力達峰值下降至某一值后趨于平穩(wěn),呈現(xiàn)出流變軟化特征;根據(jù)熱加工圖,獲得電解鎳較佳的熱加工工藝范圍為:變形溫度980~1040 ℃,應變速率3.16~10 s-1;變形溫度為1100 ℃,應變速率為1~4 s-1。"/>

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均勻化工業(yè)電解鎳高溫熱變形行為的研究
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1.蘭州理工大學 材料科學與工程學院;2.金川集團鎳合金有限公司

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甘肅省科技重大專項(22ZD6GA008);甘肅省科技計劃項目重點研發(fā)計劃(21YF5GD186);甘肅省高等學校產(chǎn)業(yè)支撐計劃項目(2022CYZC-19);蘭州理工大學省部共建有色金屬先進加工與再利用國家重點實驗室開放基金(SKLAB02019012)


Study of high-temperature hot deformation behavior of electrolytic nickel in homogenized industy
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School of Materials Science and Engineering,Lanzhou University of Technology

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    摘要:

    采用Gleeble-3500熱模擬試驗機對均勻化后的工業(yè)電解鎳進行了熱壓縮實驗,在變形量60%的條件下,研究了變形溫度為900,1000,1100,1200 ℃,應變速率為0.01,0.1,1,10 s-1時的熱變形行為。根據(jù)壓縮數(shù)據(jù)獲得真應力-真應變曲線,分析了變形溫度和應變速率對電解鎳力學性能的影響,并得到流變應力本構方程,基于動態(tài)材料模型及Prassd失穩(wěn)準則建立了熱加工圖。結果表明:電解鎳對變形溫度和應變速率表現(xiàn)出較強的敏感性,隨變形溫度的升高和應變速率的降低,流變應力逐漸減?。浑S應變的增加,流變應力達峰值下降至某一值后趨于平穩(wěn),呈現(xiàn)出流變軟化特征;根據(jù)熱加工圖,獲得電解鎳較佳的熱加工工藝范圍為:變形溫度980~1040 ℃,應變速率3.16~10 s-1變形溫度為1100 ℃,應變速率為1~4 s-1。

    Abstract:

    Hot deformation experiments were carried out on homogenized industrial electrolytic nickel using a Gleeble-3500 hot simulation tester, and the hot deformation behaviors were investigated at deformation temperatures of 900, 1000, 1100, and 1200 °C, and at strain rates of 0.01, 0.1, 1, and 10s-1 at a deformation amount of 60%.The true stress-true strain curves were obtained based on the compression data, the effects of deformation temperature and strain rate on the mechanical properties of electrolytic nickel were analyzed, and the rheological stress eigenstructure equations were obtained, and the thermal processing diagrams were established based on the dynamic material model and the Prassd instability criterio.The results show that electrolytic nickel exhibits strong sensitivity to deformation temperature and strain rate, and the rheological stress decreases gradually with the increase of deformation temperature and the decrease of strain rate;The rheological stress reaches a peak and decreases to a certain value and then tends to stabilize, showing the characteristics of rheological softening;According to the thermal processing diagram, the better thermal processing range of electrolytic nickel is obtained as follows: deformation temperature 980~1040 °C, strain rate 3.16~10s-1; deformation temperature 1100 °C, strain rate 1~4 s-1.

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張涵,桑晨,喬及森,徐仰濤,苗成鵬,李淵,劉曉波,禹澤海,董生茂,夏天東.均勻化工業(yè)電解鎳高溫熱變形行為的研究[J].稀有金屬材料與工程,2024,53(9):2661~2668.[Zhang Han, Sang Chen, Qiao Jisen, Xu Yangtao, Miao Chengpeng, Li Yuan, Liu Xiaobin, Yu Zehai, Dong Shengmao, Xia Tiandong. Study of high-temperature hot deformation behavior of electrolytic nickel in homogenized industy[J]. Rare Metal Materials and Engineering,2024,53(9):2661~2668.]
DOI:10.12442/j. issn.1002-185X.20230502

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  • 收稿日期:2023-08-15
  • 最后修改日期:2023-11-09
  • 錄用日期:2023-11-17
  • 在線發(fā)布日期: 2024-09-13
  • 出版日期: 2024-09-04