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Mg-Gd-Y-Zn-Zr合金旋轉(zhuǎn)反擠壓杯形件的組織演變和動(dòng)態(tài)再結(jié)晶機(jī)制
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中北大學(xué) 材料科學(xué)與工程學(xué)院

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國(guó)家自然科學(xué)基金(52075501); 國(guó)家自然科學(xué)基金(52205428);山西省基礎(chǔ)研究計(jì)劃資助項(xiàng)目(20210302124206)


Organization evolution and dynamic recrystallization mechanism of Mg-Gd-Y-Zn-Zr alloy rotationally counter-extruded cuprates
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North University of China,Taiyuan

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    摘要:

    本文使用傳統(tǒng)反擠壓(Conventional Backward Extrusion,CBE)和旋轉(zhuǎn)反擠壓(Rotational Backward Extrusion,RBE)兩種工藝制備了不同的Mg-9Gd-4Y-2Zn-0.5Zr (wt.%)合金杯形件。使用OM、SEM、EBSD等測(cè)試方法對(duì)不同杯形件的對(duì)應(yīng)區(qū)域進(jìn)行表征。結(jié)果表明:RBE的晶粒細(xì)化能力遠(yuǎn)遠(yuǎn)大于CBE,RBE心部的晶粒細(xì)化效果最好,RBE-Ⅲ區(qū)域的動(dòng)態(tài)再結(jié)晶(Dynamic Recrystallization,DRX)含量可達(dá)98.1%,平均晶粒尺寸為2.5μm。RBE的織構(gòu)弱化能力也優(yōu)于CBE,心部的織構(gòu)強(qiáng)度可弱化為1.258。在RBE得到杯形件當(dāng)中,其LPSO相的破碎程度也大于CBE,第二相(β相)分布的也更加均勻,析出的β相可以通過(guò)粒子刺激形核(Particles Simulated Nucleation,PSN)機(jī)制促進(jìn)DRX,并通過(guò)釘扎效應(yīng)抑制晶粒長(zhǎng)大。在CBE和RBE杯形件成形過(guò)程中,其動(dòng)態(tài)再結(jié)晶機(jī)制相同,為連續(xù)動(dòng)態(tài)再結(jié)晶(Continuous Dynamic ecrystallization,CDRX)和不連續(xù)動(dòng)態(tài)再結(jié)晶(Discontinuous Dynamic Recrystallization,DDRX)兩種。

    Abstract:

    In this paper, different cuprates of Mg-9Gd-4Y-2Zn-0.5Zr (wt.%) alloys were prepared using Conventional Backward Extrusion (CBE) and Rotational Backward Extrusion (RBE) processes. The corresponding regions of the different cuprates were characterized using OM, SEM, EBSD and other testing methods. The results show that the grain refining ability of RBE is much larger than that of CBE, and the grain refining effect in the heart of RBE is the best, and the content of Dynamic Recrystallization (DRX) in the RBE-III region can be up to 98.1%, with an average grain size of 2.5 μm. The texture weakening ability of RBE is also better than that of CBE, and the texture strength of the core can be weakened to 1.258. In the RBE cups, the degree of crushing of the LPSO phase is also larger than that of CBE, and the distribution of the second phase (β-phase) is more uniform, and the precipitated β-phase can promote DRX through the mechanism of Particles Simulated Nucleation (PSN) and restrain the growth of the grains through the pinning effect. In CBE and RBE cup molding processes, the dynamic recrystallization mechanism is the same, which is Continuous Dynamic Recrystallization (CDRX) and Discontinuous Dynamic Recrystallization (DDRX).

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徐健,喬為棟,閆釗鳴,薛勇. Mg-Gd-Y-Zn-Zr合金旋轉(zhuǎn)反擠壓杯形件的組織演變和動(dòng)態(tài)再結(jié)晶機(jī)制[J].稀有金屬材料與工程,2024,53(9):2653~2660.[Xu Jian, Qiao Weidong, Yan Zhaoming, Xue Yong. Organization evolution and dynamic recrystallization mechanism of Mg-Gd-Y-Zn-Zr alloy rotationally counter-extruded cuprates[J]. Rare Metal Materials and Engineering,2024,53(9):2653~2660.]
DOI:10.12442/j. issn.1002-185X.20230497

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  • 收稿日期:2023-08-13
  • 最后修改日期:2023-12-09
  • 錄用日期:2024-01-05
  • 在線發(fā)布日期: 2024-09-13
  • 出版日期: 2024-09-04