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超細(xì)晶擠壓態(tài)FGH4113A高溫合金等溫鍛造過程中的本構(gòu)特性及組織演變
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1.深圳市萬澤中南研究院有限公司;2.深圳市萬澤中南研究院有限公司, 深圳市萬澤航空科技有限責(zé)任公司, 中南大學(xué)粉末冶金研究院;3.深圳市萬澤中南研究院有限公司, 中南大學(xué)粉末冶金研究院;4.深圳市萬澤中南研究院有限公司, 深圳市萬澤航空科技有限責(zé)任公司

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國家科技重大專項(xiàng)(2017-VI-0009-0080); 深圳市工業(yè)和信息化局項(xiàng)目(201806071114243770);深圳市科技創(chuàng)新委員會(huì)項(xiàng)目(20150128085205453); 廣東省珠江人才計(jì)劃(607264877417)


Constitutive Characterization and Microstructure Evolution of an as-extruded FGH4113A Superalloy with ultrafine Grain during isothermal Forging
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    摘要:

    鍛造是先進(jìn)航空發(fā)動(dòng)機(jī)粉末渦輪盤制備的關(guān)鍵成型工藝。合金的化學(xué)成分和擠壓工藝很大程度上決定了擠壓態(tài)合金的組織。新型鎳基粉末高溫合金FGH4113A(WZ-A3)熱擠壓之后晶粒度達(dá)到13級(jí)以上,擠壓態(tài)合金呈現(xiàn)γ+γ"雙相組織。細(xì)小均勻的雙相組織為更為廣闊的等溫鍛造工藝窗口提供可能。本研究采用超細(xì)晶擠壓態(tài)合金FGH4113A進(jìn)行溫度分別為1000,1040,1080,1120℃;應(yīng)變速率為0.001,0.01,0.1s-1的Gleeble熱壓縮試驗(yàn),壓縮量為60%。試驗(yàn)結(jié)果表明合金試樣在所有壓縮條件下均未發(fā)生開裂,體現(xiàn)超細(xì)晶擠壓態(tài)合金FGH4113A有廣闊的等溫鍛造工藝窗口。合金的平均激活能僅為515.375kJ/mol。慢應(yīng)變速率下(0.001s-1),試樣真應(yīng)力-真應(yīng)變曲線呈現(xiàn)出穩(wěn)態(tài)流變特性;快應(yīng)變速率下(0.1s-1),試樣的真應(yīng)力-真應(yīng)變曲線呈現(xiàn)出加工硬化到再結(jié)晶軟化的變化。γ"對(duì)變形溫度敏感,高的變形溫度會(huì)引發(fā)γ"的溶解而導(dǎo)致再結(jié)晶晶粒的長大。此外,研究發(fā)現(xiàn)超細(xì)晶擠壓態(tài)合金FGH4113A在等溫鍛造過程中主要再結(jié)晶方式為不連續(xù)動(dòng)態(tài)再結(jié)晶。本研究為超細(xì)晶擠壓態(tài)合金FGH4113A的鍛造工藝制定提供了試驗(yàn)依據(jù)。

    Abstract:

    Forging is the key forming process for producing advanced aero-engine powder turbine disks. The microstructure of as-extruded alloy mostly depends on the chemical composition of alloy and extrusion processing parameters. Average grain size number is greater than 13 for the novel powder nickel-based superalloy FGH4113A after hot extrusion. As-extruded alloy has two phases microstructure of γ+γ". Fine homogenization two phases microstructure makes it possible to broaden isothermal forging processing window. In this study, Gleeble hot compression experiments for as-extruded FGH4113A alloy with ultrafine grains were carried out at temperatures of 1000, 1040, 1080, 1120℃ and strain rates of 0.001, 0.01, 0.1s-1. Height reduction is 60% for samples under all experiment conditions. The results show that no crack was found on the surface of alloy samples under all experiment conditions, suggesting as-extruded FGH4113A alloy with ultrafine grains has a wide isothermal forging process window. The average activation energy for the alloy is 515.375kJ/mol. True stress-true strain curves show steady flow characteristic for samples with slow strain rate (0.001s-1) and the change from work hardening to recrystallization softening for samples with fast strain rate (0.1s-1). γ" is sensitive to temperature. Recrystallization grains grow obviously at high deformation temperature due to the large amount of dissolution of γ". Furthermore, the study shows that the main recrystallization way is discontinuous dynamic recrystallization for as-extruded FGH4113A alloy with ultrafine grains. This study offers experiment evidence for designing forging processing of the as-extruded FGH4113A alloy with ultrafine grains.

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李遠(yuǎn),何英杰,馬向東,楊金龍,郭建政,馮干江.超細(xì)晶擠壓態(tài)FGH4113A高溫合金等溫鍛造過程中的本構(gòu)特性及組織演變[J].稀有金屬材料與工程,2024,53(8):2275~2284.[Li Yuan, He Yingjie, Ma Xiangdong, Yang Jinlong, Guo Jianzheng, Feng Ganjiang. Constitutive Characterization and Microstructure Evolution of an as-extruded FGH4113A Superalloy with ultrafine Grain during isothermal Forging[J]. Rare Metal Materials and Engineering,2024,53(8):2275~2284.]
DOI:10.12442/j. issn.1002-185X.20230416

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  • 收稿日期:2023-07-02
  • 最后修改日期:2023-07-30
  • 錄用日期:2023-08-24
  • 在線發(fā)布日期: 2024-08-20
  • 出版日期: 2024-08-08