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等通道轉(zhuǎn)角擠壓對Mg-1Gd、Mg-2Zn二元合金的組織及力學(xué)性能的影響
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作者單位:

1.山東科技大學(xué)材料科學(xué)與工程學(xué)院;2.中國科學(xué)院金屬研究所 師昌緒先進(jìn)材料創(chuàng)新中心

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基金項(xiàng)目:

國家自然科學(xué)基金(Nos. 52271107);山東省自然科學(xué)基金(No. ZR2021ME241)


Effect of equal channel angular extrusion on microstructure and mechanical properties of Mg-1Gd and Mg-2Zn alloys
Author:
Affiliation:

1.School of Materials Science and Engineering,Shandong University of Science and Technology;2.Shi-changxu Innovation Center for Advanced Materials,Institute of Metal Research,Chinese Academy of Sciences

Fund Project:

National Natural Science Foundation of China (Nos. 52271107); Shandong provincial Natural Science Foundation (No. ZR2021ME241)

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    摘要:

    本文使用金相、EBSD等手段研究了等通道擠壓對Mg-1Gd、Mg-2Zn兩種二元合金組織和力學(xué)性能的影響。結(jié)果表明,在相同擠壓條件下,Mg-2Zn合金發(fā)生完全再結(jié)晶,晶粒長大粗化,且強(qiáng)度塑性不隨著擠壓道次變化;Mg-1Gd合金則只發(fā)生了部分動態(tài)再結(jié)晶,組織為細(xì)小的動態(tài)再結(jié)晶晶粒和變形晶粒,伴隨擠壓道次的增加,再結(jié)晶程度提升,合金的抗拉強(qiáng)度與塑性增加了一倍。這與溶質(zhì)原子Gd比Zn更能抑制再結(jié)晶和晶粒長大有關(guān)。Mg-1Gd合金的再結(jié)晶晶粒的取向分散,而未再結(jié)晶的晶粒c軸取向由ED向TD偏轉(zhuǎn)45°,這與宏觀織構(gòu)的檢測相互印證,晶粒內(nèi)部產(chǎn)生大量的小角度晶界,小角度晶界兩側(cè)發(fā)生圍繞c軸的轉(zhuǎn)動,并逐漸演化為大角度晶界。

    Abstract:

    This article uses metallographic and EBSD techniques to study the effects of equal channel angular pressing on the microstructure and mechanical properties of two binary alloys, Mg-1Gd and Mg-2Zn. The results show that under the same pressing conditions, Mg-2Zn alloy fully recrystallized, resulting in grain growth and coarsening, and the strength and plasticity did not change with the number of pressing passes. Mg-1Gd alloy only partially recrystallized after pressing, with a microstructure consisting of fine dynamic recrystallized grains and deformed grains. With an increase in the number of pressing passes, the degree of recrystallization increased, leading to a doubling of the alloy"s tensile strength and plasticity. This was related to the greater inhibition of recrystallization and grain growth by the solute atom Gd compared to Zn. The recrystallized grains had a dispersed orientation, while the grains that did not recrystallize in Mg-1Gd alloy had a c-axis orientation that deviated 45° from ED to TD, which was consistent with the detection of macroscopic texture. A large number of small-angle grain boundaries formed within the grains, and rotations around the c-axis occurred on both sides of these boundaries, gradually evolving into large-angle boundaries.

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引用本文

許金良,宋宜帆,丁睿智,閆宏,陳榮石.等通道轉(zhuǎn)角擠壓對Mg-1Gd、Mg-2Zn二元合金的組織及力學(xué)性能的影響[J].稀有金屬材料與工程,2024,53(6):1735~1740.[Xu Jin-liang, Song Yi-fan, Ding Rui-zhi, Yan Hong, Chen Rong-shi. Effect of equal channel angular extrusion on microstructure and mechanical properties of Mg-1Gd and Mg-2Zn alloys[J]. Rare Metal Materials and Engineering,2024,53(6):1735~1740.]
DOI:10.12442/j. issn.1002-185X.20230223

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  • 收稿日期:2023-04-19
  • 最后修改日期:2023-12-25
  • 錄用日期:2024-01-05
  • 在線發(fā)布日期: 2024-06-24
  • 出版日期: 2024-06-17