14 m-2下降到4.2×1013 m-2,大角度晶界含量從63.8%增加到70.8%,使得位錯(cuò)湮滅速率提升,從而導(dǎo)致了應(yīng)變硬化能力的降低。在90~210 ℃的強(qiáng)磁場(chǎng)退火條件下,低含量的大角度晶界(61.7%~66.2%)可以提供一個(gè)較慢的位錯(cuò)湮滅速率,從而導(dǎo)致較高的均勻延伸率(0.64%~1.60%)和更慢的屈服點(diǎn)后的流變應(yīng)力下降。"/>

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低溫等徑角擠壓制備1050鋁合金在磁退火后的均勻延伸率和屈服下降現(xiàn)象
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1.東北大學(xué) 材料電磁過程研究教育部重點(diǎn)實(shí)驗(yàn)室,遼寧 沈陽(yáng) 110819;2.東北大學(xué) 材料科學(xué)與工程學(xué)院,遼寧 沈陽(yáng) 110819

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基金項(xiàng)目:

National Natural Science Foundation of China (No. 51574076)


Uniform Elongation and Yield-Drop Phenomenon in Magnetically Annealed 1050 Aluminum Alloy Prepared by CryoECAP
Author:
Affiliation:

1.Key Lab of Electromagnetic Processing of Materials, Ministry of Education, Northeastern University, Shenyang 110819, China;2.School of Materials Science and Engineering, Northeastern University, Shenyang 110819, China

Fund Project:

National Natural Science Foundation of China (51574076)

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    摘要:

    采用低溫等徑角擠壓(cryoECAP)制備了超細(xì)晶(UFG)1050鋁合金。采用拉伸試驗(yàn)、透射電子顯微鏡和電子背散射衍射等方法,研究了UFG 1050鋁合金在90~210 ℃、無(wú)磁場(chǎng)和12 T強(qiáng)磁場(chǎng)下退火4 h后的拉伸行為和顯微組織。1050鋁合金經(jīng)cryoECAP退火后,晶粒尺寸為0.70~1.28 μm,極限抗拉伸強(qiáng)度與屈服強(qiáng)度之比小于1.24,均勻延伸率小于2.3%。隨著退火溫度從90 ℃上升到210 ℃,屈服下降現(xiàn)象變得明顯,這是因?yàn)樵诶熳冃芜^程中,為了維持所施加的應(yīng)變速率,可動(dòng)位錯(cuò)有所減少。均勻延伸率從1.55%下降到0.55%,位錯(cuò)密度從5.6×1014 m-2下降到4.2×1013 m-2,大角度晶界含量從63.8%增加到70.8%,使得位錯(cuò)湮滅速率提升,從而導(dǎo)致了應(yīng)變硬化能力的降低。在90~210 ℃的強(qiáng)磁場(chǎng)退火條件下,低含量的大角度晶界(61.7%~66.2%)可以提供一個(gè)較慢的位錯(cuò)湮滅速率,從而導(dǎo)致較高的均勻延伸率(0.64%~1.60%)和更慢的屈服點(diǎn)后的流變應(yīng)力下降。

    Abstract:

    The ultrafine grained (UFG) 1050 aluminum alloy was prepared by equal channel angular pressing at cryogenic temperature, namely cryoECAP process. The tensile behavior and microstructures of UFG 1050 aluminum alloy after annealing at 90–210 °C for 4 h without and with high magnetic field of 12 T were investigated by tensile tests, transmission electron microscope, and electron backscattered diffraction analyses. After cryoECAP and annealing treatments, the 1050 aluminum alloy has ultrafine grains with 0.7–1.28 μm in size, the ratio of ultimate tensile strength to yield strength is less than 1.24, and the uniform elongation is less than 2.3%. With increasing the annealing temperature from 90 °C to 210 °C, the yield-drop phenomenon becomes more obvious due to the decrease in mobile dislocations to maintain the applied strain rate during tensile deformation. The uniform elongation decreases from 1.55% to 0.55%, the dislocation density reduces from 5.6×1014 m-2 to 4.2×1013 m-2, and the fraction of high-angle grain boundaries (HABs) increases from 63.8% to 70.8%. These phenomena cause the higher annihilation rate of dislocations, thereby leading to the degradation of strain hardening effect. During annealing under high magnetic field at 90–210 °C, the low fraction of HABs (61.7%–66.2%) can provide a slower annihilation rate of dislocations, therefore resulting in the higher uniform elongation (0.64%–1.60%) and slower decrease in the flow stress after the yield peak.

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何立子,陳健,陳慶倫,韓寧,李力爽,王美洋,王宇欽.低溫等徑角擠壓制備1050鋁合金在磁退火后的均勻延伸率和屈服下降現(xiàn)象[J].稀有金屬材料與工程,2023,52(9):2993~3002.[He Lizi, Chen Jian, Chen Qinglun, Han Ning, Li Lishuang, Wang Meiyang, Wang Yuqin. Uniform Elongation and Yield-Drop Phenomenon in Magnetically Annealed 1050 Aluminum Alloy Prepared by CryoECAP[J]. Rare Metal Materials and Engineering,2023,52(9):2993~3002.]
DOI:10.12442/j. issn.1002-185X.20230217

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  • 收稿日期:2023-04-17
  • 最后修改日期:2023-05-19
  • 錄用日期:2023-05-30
  • 在線發(fā)布日期: 2023-09-22
  • 出版日期: 2023-09-21