拉伸孿晶形式存在。隨著應(yīng)力幅值的增加晶粒逐漸細(xì)化,這是由于在循環(huán)過(guò)程中,拉伸孿晶演變誘導(dǎo)晶粒細(xì)化。隨著應(yīng)力幅值的增加,織構(gòu)強(qiáng)度顯著減弱,這與試樣疲勞后的再結(jié)晶機(jī)制有關(guān)。通過(guò)對(duì)試樣疲勞斷口的分析,發(fā)現(xiàn)孿晶片層處容易引起裂紋萌生,隨著應(yīng)力的增加,試樣中裂紋擴(kuò)展區(qū)面積逐漸減小,在疲勞裂紋擴(kuò)展區(qū)觀察到明顯的疲勞輝紋。最終斷裂區(qū)表面粗糙,主要存在韌窩、撕裂脊以及二次裂紋等形貌。在最終斷裂區(qū)可觀察到韌窩,韌窩尺寸隨著循環(huán)應(yīng)力的增加,在較高加載頻率下,韌窩的尺寸與數(shù)量均減小。"/>

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AZ31鎂合金在高周疲勞過(guò)程中微觀組織和孿晶演變特征
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作者單位:

1.北京航空航天大學(xué) 材料科學(xué)與工程學(xué)院,北京 100191;2.中北大學(xué) 材料科學(xué)與工程學(xué)院,山西 太原 030051

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基金項(xiàng)目:

國(guó)家自然科學(xué)基金資助項(xiàng)目(U1764253); 山西省自然科學(xué)基金資助項(xiàng)目(201901D111167);


Evolution Characteristics of Microstructure and Twin in High-Cycle Fatigue of AZ31 Magnesium Alloy
Author:
Affiliation:

1.School of Materials Science and Engineering, Beihang University, Beijing 100191, China;2.School of Materials Science and Engineering, North University of China, Taiyuan 030051, China

Fund Project:

國(guó)家自然科學(xué)基金資助項(xiàng)目(U1764253); 山西省自然科學(xué)基金資助項(xiàng)目(201901D111167);

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    摘要:

    利用掃描電子顯微鏡(SEM)和電子背散射衍射(EBSD)技術(shù)研究了室溫條件下AZ31鎂合金在不同加載頻率(3和30 Hz)和不同應(yīng)力幅值(90,95,100,105,110 MPa)疲勞變形后的組織演變規(guī)律及斷口形貌特征。結(jié)果表明:隨著加載應(yīng)力增加,基體內(nèi)殘余孿晶數(shù)量增加,殘余孿晶主要以拉伸孿晶形式存在。隨著應(yīng)力幅值的增加晶粒逐漸細(xì)化,這是由于在循環(huán)過(guò)程中,拉伸孿晶演變誘導(dǎo)晶粒細(xì)化。隨著應(yīng)力幅值的增加,織構(gòu)強(qiáng)度顯著減弱,這與試樣疲勞后的再結(jié)晶機(jī)制有關(guān)。通過(guò)對(duì)試樣疲勞斷口的分析,發(fā)現(xiàn)孿晶片層處容易引起裂紋萌生,隨著應(yīng)力的增加,試樣中裂紋擴(kuò)展區(qū)面積逐漸減小,在疲勞裂紋擴(kuò)展區(qū)觀察到明顯的疲勞輝紋。最終斷裂區(qū)表面粗糙,主要存在韌窩、撕裂脊以及二次裂紋等形貌。在最終斷裂區(qū)可觀察到韌窩,韌窩尺寸隨著循環(huán)應(yīng)力的增加,在較高加載頻率下,韌窩的尺寸與數(shù)量均減小。

    Abstract:

    Microstructure evolution and fracture morphology during high cycle fatigue in AZ31 magnesium alloy were investigated by fatigue test at different loading frequencies (3 and 30 Hz) and stress amplitudes (90, 95, 100, 105, 110 MPa). Electron back-scattered diffraction (EBSD) analysis results show that the number of residual twins in the matrix increases with the increase in loading stress, and the residual twins mainly exist in the form of {102} tensile twins. Gradual grain refinement is observed with increasing stress amplitude, which is due to the grain refinement induced by the evolution of tensile twinning during fatigue deformation. The significant weakening of the texture strength with increasing stress amplitude is related to the recrystallization mechanism after fatigue deformation. Through the scanning electron microscope (SEM) analysis of the fatigue fracture, it is found that the fatigue crack initiation (FCI) occurs in twin layer, the area of the fatigue crack growth (FCG) in the specimen gradually decreases with the increase in stress, and obvious fatigue striations (FS) are observed in FCG. The final fracture (FF) is rough surface, and there are mainly tear ridges and dimples. The dimple is observed in the final fracture, and the size and number of dimples decrease with the increase in stress.

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楊福來(lái),王強(qiáng),張崢.AZ31鎂合金在高周疲勞過(guò)程中微觀組織和孿晶演變特征[J].稀有金屬材料與工程,2023,52(8):2693~2701.[Yang Fulai, Wang Qiang, Zhang Zheng. Evolution Characteristics of Microstructure and Twin in High-Cycle Fatigue of AZ31 Magnesium Alloy[J]. Rare Metal Materials and Engineering,2023,52(8):2693~2701.]
DOI:10.12442/j. issn.1002-185X.20230116

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  • 收稿日期:2023-03-06
  • 最后修改日期:2023-07-27
  • 錄用日期:2023-04-27
  • 在線發(fā)布日期: 2023-08-25
  • 出版日期: 2023-08-24