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型殼保溫方式對一種等軸晶鎳基鑄造高溫合金組織和力學性能的影響
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1.中國科學院金屬研究所 師昌緒先進材料創(chuàng)造中心;2.貴州安吉航空精密鑄造有限責任公司

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國家自然科學基金資助(項目號52001314);國家科技重大專項資助(項目號J2019-Ⅶ-0002-0142, No. J2019-VI-0004-0118)


Effect of shell insulation methods on microstructure and mechanical properties of an equiaxed Nickel-based cast superalloy
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Shi-changxu Innovation Center for Advanced Materials,Institute of Metal Research,Chinese Academy of Sciences

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    摘要:

    通過設(shè)計型殼保溫方式改變合金凝固冷卻速率,分析了凝固冷卻速率對一種等軸晶鎳基鑄造高溫合金K4750顯微組織和室溫拉伸性能的影響。設(shè)計的四種型殼保溫方式包括填砂、試棒不包保溫氈、包單層保溫氈和包雙層保溫氈,型殼試棒處的凝固冷卻速率大小順序為:試棒不包保溫氈≥填砂>>包單層保溫氈≥包雙層保溫氈。標準熱處理后,型殼填砂的試棒室溫抗拉強度最高(1115MPa),試棒不包保溫氈次之(1095MPa),包單層保溫氈與包雙層保溫氈最差(分別為950MPa和952.5MPa)。室溫屈服強度、延伸率和斷面收縮率變化規(guī)律與室溫抗拉強度相同。采用OM、SEM以及EBSD等方法表征合金顯微組織,發(fā)現(xiàn)型殼填砂、試棒不包保溫氈、包單層保溫氈和包雙層保溫氈的試棒晶粒均為等軸晶,平均晶粒尺寸分別為176μm、167μm、325μm、315μm。填砂和試棒不包保溫氈合金凝固冷速較快,形成的細小等軸晶在應(yīng)力條件下易于協(xié)調(diào)變形,凝固過程形成的MC型一次碳化物更細小且主要呈塊狀,有利于抑制變形時微孔洞、裂紋的擴展,顯著提高了合金室溫拉伸性能。相反,型殼包單層和雙層保溫氈的合金凝固冷速較慢,形成的大尺寸等軸晶不利于晶粒間的協(xié)調(diào)變形,析出的大尺寸長條狀MC型一次碳化物促進孔洞、微裂紋的萌生與擴展,使合金室溫強度和塑性均顯著下降。

    Abstract:

    The effect of solidification cooling rate on microstructure and room temperature tensile properties of equiaxed nickel-based cast superalloy K4750 were studied by designing shell insulation methods. Four types of insulation methods were designed, including: sand-filled, test bars without insulation felt, wrapped single-layer insulation felt and wrapped double-layer insulation felt, and the order of solidification cooling rate at the test bar of the shell is: test bars without insulation felt ≥ sand-filled > > wrapped single-layer insulation felt ≥ wrapped double-layer insulation felt. After standard heat treatment, the test bar with sand-filled shell has the highest room temperature tensile strength (1115MPa), the test bar without insulation felt is the seconed highest (1095MPa), and the single-layer insulation felt and the double-layer insulation felt are the worst (950MP and 952.5MPa respectively). OM, SEM and EBSD were used to characterise the microstructure of the alloy. The results show that the grains of sand-filled, test bars without insulation felt, single-layer insulation felt and double-layer insulation felt are equiaxed crystals, and the average grain sizes were 176μm, 167μm, 325μm and 315μm, respectively. Sand-filled and test bars without insulation felt alloys solidification cooling rate is faster, the formation of small equiaxed crystals more easily coordinated deformation in the stress conditions, solidification process to form the MC type primary carbide is finer and mainly in the form of blocks, which is conducive to inhibit the expansion of microvoids and cracks during deformation, significantly improving the tensile properties of the alloy at room temperature. On the contrary, single-layer insulation felt and double-layer insulation felt alloys solidification cooling rate is slower, the formation of large-size equiaxed crystals are not conducive to the coordinated deformation between the grains, and the precipitation of MC type primary carbide with large size and long strip shape promotes the emergence and expansion of holes and microcracks, which significantly reduces the strength and plasticity of the alloy at room temperature.

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張茂源,歐美瓊,冉興,侯坤磊,曹建,馬穎澈.型殼保溫方式對一種等軸晶鎳基鑄造高溫合金組織和力學性能的影響[J].稀有金屬材料與工程,2024,53(3):757~767.[Zhang Maoyuan, Ou Meiqiong, Ran Xing, Hou Kunkei, Cao Jian, Ma Yingche. Effect of shell insulation methods on microstructure and mechanical properties of an equiaxed Nickel-based cast superalloy[J]. Rare Metal Materials and Engineering,2024,53(3):757~767.]
DOI:10.12442/j. issn.1002-185X.20230095

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  • 收稿日期:2023-02-27
  • 最后修改日期:2023-04-26
  • 錄用日期:2023-04-27
  • 在線發(fā)布日期: 2024-03-27
  • 出版日期: 2024-03-20