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工業(yè)純鈦TA1退火過(guò)程中的應(yīng)力誘導(dǎo)晶粒長(zhǎng)大行為
作者:
作者單位:

1.南京工業(yè)大學(xué) 先進(jìn)輕質(zhì)高性能材料研究中心,江蘇 南京 210009;2.哈爾濱理工大學(xué) 材料科學(xué)與化工學(xué)院,黑龍江 哈爾濱 150080

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中圖分類(lèi)號(hào):

基金項(xiàng)目:

國(guó)家自然科學(xué)基金:52271104


Abnormal Grain Growth Induced by Stress During An-nealing of Industrial Pure Titanium TA1
Author:
Affiliation:

1.Key Laboratory for Light-Weight Materials, Nanjing Tech University, Nanjing 210009, China;2.School of Materials Science and Chemical Engineering, Harbin University of Science and Technology, Harbin 150080, China

Fund Project:

國(guó)家自然科學(xué)基金:52271104

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    摘要:

    探究了應(yīng)力對(duì)純鈦再結(jié)晶行為的影響。在純鈦板的退火過(guò)程中施加彎曲應(yīng)力,并觀察一個(gè)截面在拉伸和壓縮應(yīng)力下的再結(jié)晶過(guò)程。制備了變形量分別為20%、40%和60%的工業(yè)純鈦TA1軋制板,然后將這些樣品置于600 ℃和30 MPa下保溫10 min。結(jié)果表明,在變形20%和40%的樣品中,只觀察到少數(shù)再結(jié)晶晶粒。此外,受應(yīng)力區(qū)域的平均晶粒尺寸大于無(wú)應(yīng)力區(qū)域。進(jìn)一步將變形40%的軋制薄板在600 ℃和30 MPa下保溫60和120 min,拉伸應(yīng)力區(qū)域中晶粒的異常生長(zhǎng)一直持續(xù)到達(dá)到臨界尺寸,之后晶粒停止生長(zhǎng)。再結(jié)晶過(guò)程中晶粒生長(zhǎng)的持續(xù)增加可歸因于應(yīng)力促進(jìn)的位錯(cuò)調(diào)節(jié)。具有有利條件的晶粒傾向于沿著所施加的應(yīng)力方向異常生長(zhǎng)。然而,鈦板內(nèi)的高密度殘余位錯(cuò)導(dǎo)致晶粒生長(zhǎng)的驅(qū)動(dòng)力降低,導(dǎo)致臨界尺寸的存在。這些發(fā)現(xiàn)解釋了鈦在拉伸和壓縮應(yīng)力下觀察到的不同再結(jié)晶行為。

    Abstract:

    The influence of stress on the recrystallization process of pure titanium was investigated. Bending stress was applied during the annealing process of a pure titanium plate to observe the recrystallization process under tensile and compressive stresses on one section. Industrial pure titanium TA1 rolled plates with different deformation levels of 20%, 40%, and 60% were prepared. These samples were then subjected to a temperature of 600 °C and a stress of 30 MPa for 10 min. It is found that in the samples with 20% and 40% deformation levels, only a few recrystallized grains are observed. Additionally, the average grain size in the region under stress becomes larger than that in the region without stress. To further investigate the grain growth, the rolled sheet with 40% deformation level was kept at 600 °C and 30 MPa for 60 and 120 min. It is observed that the abnormal growth of grains in the tensile stress area continues until the critical size is reached, after which they stop growing. The increased grain growth during recrystallization can be attributed to the stress-promoting dislocation adjustment. The grains with favorable conditions tend to grow abnormally along the direction of the applied stress. However, the high density of residual dislocations within the titanium plate results in a reduction in the driving force for grain growth, leading to the existence of critical size. These findings provide an explanation for different recrystallization behavior observed in titanium under tensile and compressive stresses.

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劉繼偉,李學(xué)問(wèn),房文斌.工業(yè)純鈦TA1退火過(guò)程中的應(yīng)力誘導(dǎo)晶粒長(zhǎng)大行為[J].稀有金屬材料與工程,2024,53(3):625~631.[Liu Jiwei, Li Xuewen, Fang Wenbin. Abnormal Grain Growth Induced by Stress During An-nealing of Industrial Pure Titanium TA1[J]. Rare Metal Materials and Engineering,2024,53(3):625~631.]
DOI:10.12442/j. issn.1002-185X.20230080

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歷史
  • 收稿日期:2023-02-16
  • 最后修改日期:2024-02-27
  • 錄用日期:2023-08-24
  • 在線發(fā)布日期: 2024-03-22
  • 出版日期: 2024-03-20