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650 ℃時(shí)效SP2215奧氏體耐熱鋼管的微觀組織和力學(xué)性能
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1.國(guó)家能源集團(tuán)新能源技術(shù)研究院有限公司;2.北京航空航天大學(xué);3.江蘇武進(jìn)不銹鋼股份有限公司

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TG142.1

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Microstructure and Mechanical Properties of SP2215 Austenitic Heat-resistant Steel Tube after Aging at 650 ℃
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Affiliation:

1.CHN Energy New Energy Technology Research Institute Co.Ltd.;2.JiangSu WuJin Stainless Steel Pipe Group Co.Ltd.

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    摘要:

    通過(guò)OM、SEM、TEM和顯微硬度、室溫沖擊以及高溫拉伸試驗(yàn),研究了650 ℃時(shí)效不同時(shí)間后SP2215奧氏體耐熱鋼管的微觀組織、力學(xué)性能及斷裂機(jī)理。結(jié)果表明,固溶態(tài)SP2215鋼微觀組織由奧氏體,少量孿晶及未溶NbN和Z相組成;650 ℃時(shí)效時(shí)Cr23C6優(yōu)先在奧氏體晶界析出,且隨時(shí)效時(shí)間延長(zhǎng)逐漸增多、粗化并形成連續(xù)網(wǎng)狀;球形富Cu相在奧氏體晶內(nèi)析出且尺寸穩(wěn)定,時(shí)效2012 h約為15 nm;SP2215鋼晶內(nèi)室溫顯微硬度在時(shí)效50 h時(shí)基本達(dá)到最大值,之后趨于穩(wěn)定,這與穩(wěn)定富Cu相的析出強(qiáng)化作用有關(guān);SP2215鋼具有明顯的高溫時(shí)效脆化傾向,時(shí)效2012 h室溫沖擊吸收功較固溶態(tài)降低約78.5%,室溫沖擊斷裂隨時(shí)效時(shí)間延長(zhǎng)由韌性斷裂向沿晶脆性斷裂轉(zhuǎn)變,這是由Cr23C6在奧氏體晶界析出并逐漸聚集、粗化導(dǎo)致的。SP2215鋼在650 ℃,2.5×10-4 s-1應(yīng)變速率下拉伸時(shí)出現(xiàn)鋸齒流變(Portevin-Le Chatelier, PLC)現(xiàn)象,鋸齒類型為T(mén)ype(A+B),隨時(shí)效時(shí)間延長(zhǎng)PLC逐漸“減弱”,但鋸齒類型不變;隨時(shí)效時(shí)間延長(zhǎng)SP2215鋼高溫拉伸屈服強(qiáng)度基本保持穩(wěn)定,抗拉強(qiáng)度和斷面收縮率逐漸降低,高溫拉伸斷裂由韌性斷裂向準(zhǔn)解理脆性斷裂轉(zhuǎn)變。

    Abstract:

    The microstructure, mechanical properties and fracture mechanism of SP2215 austenitic heat-resistant steel tube after aging at 650 ℃ for different times were studied by OM, SEM, TEM, microhardness, room temperature impact and high temperature tensile tests. The results show that the microstructure of solid solution treated SP2215 steel is composed of austenite, a small amount of twins and undissolved NbN and Z phases. Cr23C6 preferentially precipitates at austenite grain boundaries during aging at 650 ℃, and gradually increases, coarsens and forms a continuous network with the extension of aging time. The spherical Cu-rich phase is precipitated in the austenite grains, when the aging time reaching 2012 h, the size of Cu-rich phase is about 15 nm. The room temperature microhardness in grains of SP2215 steel reaches the maximum value after aging for 50 h, and then tends to be stable, which is related to the precipitation strengthening effect of stable Cu-rich phase. SP2215 steel has obvious tendency of high temperature aging embrittlement. The room temperature impact absorption energy of sample aging for 2012 h is about 78.5 % lower than that of solid solution treated sample. The impact fracture mechanism at room temperature changes from ductile fracture to intergranular brittle fracture with the extension of aging time, which is caused by the precipitation, aggregation and coarsening of Cr23C6 at austenite grain boundary. Portevin-Le Chatelier (PLC) appears when SP2215 steel was stretched with the strain rate of 2.5×10-4 s-1 at 650 ℃, and the serrated type is Type ( A + B ). With the increase of aging time, the PLC gradually “weakens”, but the serrated type remains unchanged. With the extension of aging time, the high temperature tensile yield strength of SP2215 steel remains basically stable, the tensile strength and reduction of area gradually decrease, and the high temperature tensile fracture mechanism changes from ductile fracture to quasi cleavage brittle fracture.

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靳曉坤,張世超,杜晉峰,梁軍,宋建新,張崢.650 ℃時(shí)效SP2215奧氏體耐熱鋼管的微觀組織和力學(xué)性能[J].稀有金屬材料與工程,2024,53(2):501~508.[Jin Xiaokun, Zhang Shichao, Du Jinfeng, Liang Jun, Song Jianxin, Zhang Zheng. Microstructure and Mechanical Properties of SP2215 Austenitic Heat-resistant Steel Tube after Aging at 650 ℃[J]. Rare Metal Materials and Engineering,2024,53(2):501~508.]
DOI:10.12442/j. issn.1002-185X.20230041

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歷史
  • 收稿日期:2023-01-29
  • 最后修改日期:2023-03-14
  • 錄用日期:2023-03-16
  • 在線發(fā)布日期: 2024-02-28
  • 出版日期: 2024-02-23