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GH4151合金的凝固偏析行為及均勻化熱處理研究
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“航空發(fā)動(dòng)機(jī)與燃?xì)廨啓C(jī)”國(guó)家科技重大專項(xiàng)項(xiàng)目(No.2019-Ⅵ-0006-0120);國(guó)家重點(diǎn)研發(fā)計(jì)劃項(xiàng)目(Nos.2019YFA0705300和 2017YFA0700703);中國(guó)科學(xué)院金屬研究所創(chuàng)新(No.2021-PY09);遼寧省博士啟動(dòng)(項(xiàng)目號(hào)No.2020-BS-007)


Research on solidification segregation behavior and homogenization heat treatment of GH4151 alloy
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    摘要:

    GH4151合金是一種承溫能力高達(dá)800 ℃的新型渦輪盤用鑄鍛變形高溫合金,該合金在凝固過(guò)程中元素偏析嚴(yán)重,主要偏析元素包括Nb、Mo和Ti等元素,同時(shí)合金中包含大量的C元素,在熔煉凝固后期由于殘余液相中的元素富集,枝晶間會(huì)析出大量有害相,包括(γ-γ′)共晶,Laves相,η相和MC碳化物。實(shí)驗(yàn)通過(guò)研究C含量對(duì)各偏析元素的影響發(fā)現(xiàn),增加C含量可減輕Nb元素在枝晶間的偏析,此外,隨C含量的增加枝晶更發(fā)達(dá),枝晶間區(qū)域減少。隨后通過(guò)研究在1160 ℃-1210 ℃不同溫度下的均勻化熱處理對(duì)各枝晶間析出相的影響發(fā)現(xiàn),(γ-γ′)共晶和Laves相的熔點(diǎn)約為1180 ℃,η相的熔點(diǎn)約為1200 ℃,MC碳化物的熔點(diǎn)超過(guò)1300 ℃;同時(shí),發(fā)現(xiàn)1170 ℃/16 h- 1200 ℃/8 h雙步均勻化熱處理不僅可以消除鑄錠中的偏析,而且避免了低熔點(diǎn)相過(guò)燒而產(chǎn)生的孔洞,使坯料更加有利于后續(xù)開坯變形。

    Abstract:

    GH4151 alloy is a new type of casting and deformation superalloy of turbine disk with the temperature bearing capacity up to 800 ℃. The alloy has severe elemental segregation during solidification, main segregation elements including Nb, Ti and Mo element. Meanwhile, the alloy contains a large amount of C element. In the late stages of solidification, due to the enrichment of elements in the residual liquid phase, a large number of harmful phases, including (γ-γ′) eutectic, Laves phase, η phase and MC carbides, precipitate between the dendrites. By studying the influence of C content on the segregation elements, it is found that increasing C content can reduce the segregation of Nb elements between dendrites. In addition, with the increase of C content, the dendrites become more developed and the inter-dendrite area decreases. The melting points were determined by studying the effects of homogenization heat treatment at different temperatures from 1160 ℃ to 1210 ℃ that (γ-γ") eutectic and Laves phases are about 1180 ℃, η phase is about 1200 ℃ and MC carbide is more than 1300 ℃. At the same time, it is found that the 1170 ℃/16 h-1200 ℃/8 h double step homogenization heat treatment can not only eliminate the segregation in the ingot, but also avoid the holes caused by the overburning of the low melting point phases, which makes the billet more conducive to the subsequent billet deformation.

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蓋永超,張瑞,周子薦,呂少敏,崔傳勇,曲敬龍. GH4151合金的凝固偏析行為及均勻化熱處理研究[J].稀有金屬材料與工程,2024,53(1):159~168.[Gai Yongchao, Zhang Rui, Zhou Zijian, Lv Shaomin, Cui Chuanyong, Qu Jinglong. Research on solidification segregation behavior and homogenization heat treatment of GH4151 alloy[J]. Rare Metal Materials and Engineering,2024,53(1):159~168.]
DOI:10.12442/j. issn.1002-185X.20220996

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  • 收稿日期:2022-12-23
  • 最后修改日期:2023-02-08
  • 錄用日期:2023-02-21
  • 在線發(fā)布日期: 2024-01-29
  • 出版日期: 2024-01-24