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變形參數(shù)對FGH4113A粉末高溫合金微觀組織演化的影響
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國家科技重大專項(2017-Ⅵ-0009-0080);廣東省重點領域研發(fā)計劃項目(2019B010935001);深圳市海外高層次人才資金(KQTD2015032716463668);深圳市科技計劃資助 JSGG20210802093205015


Effect of Deformation Parameters on Microstructure Evolution of FGH4113A Powder Metallurgy Superalloy
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    摘要:

    本文針對一種新型粉末高溫合金FGH4113A(WZ-A3)進行了一系列熱壓縮實驗,探究了變形溫度、應變速率、應變量對微觀組織演化的影響規(guī)律,并提出了獲得細小均勻“γ+γ′雙相晶粒組織”的熱變形參數(shù)。結(jié)果表明:在溫度1100 ℃、應變速率0.1 s-1、真應變0.1~0.7范圍內(nèi),應變增大有利于促進動態(tài)再結(jié)晶以及細化晶粒。隨應變增加,γ"相體積分數(shù)先減小后增大,隨后保持穩(wěn)定,并且在熱變形過程中γ"相形貌逐漸趨于球形。在溫度1100 ℃、變形量50%、應變速率0.01~1 s-1范圍內(nèi),應變速率增大能夠提高動態(tài)再結(jié)晶程度并細化晶粒。應變速率由0.01~0.1 s-1增大至1 s-1時,由于絕熱溫升以及位錯滑移加劇,γ"相體積分數(shù)減小約2%。在應變速率0.1 s-1、變形量50%、溫度1070~1160 ℃范圍內(nèi),變形溫度的提升有利于促進動態(tài)再結(jié)晶和晶粒長大。隨著變形溫度升高至1130 ℃,γ"相已大量溶解,釘扎晶界能力大幅減弱,平均晶粒尺寸增大至12.1 μm。在變形溫度1100 ℃、應變速率1 s-1、50%變形量條件下可以獲得均勻細小的“γ+γ′雙相晶粒組織”,晶粒度能夠達到12級以上。

    Abstract:

    Through a series of hot compression tests on a novel powder metallurgy superalloy FGH4113A (WZ-A3), the effects of deformation temperature, strain rate and strain on the microstructure evolution were investigated. The results demonstrate that when the temperature is 1100 ℃, the strain rate is 0.1 s-1 and the true strain is 0.1~0.7, the increase of strain is beneficial to promote dynamic recrystallization and grain refinement. With the increase of strain, the volume fraction of γ" phase first decreases, then increases, and eventually remains stable. The morphology of γ" phase gradually becomes spherical during the thermal deformation process. Under the conditions of temperature 1100 ℃, deformation 50% and strain rate of 0.01~1 s-1, the increase of strain rate can improve the degree of dynamic recrystallization and refine the grains. With the increase of strain rate from 0.01~0.1 s-1 to 1 s-1, adiabatic temperature rise and dislocation slip intensify, resulting in the volume fraction of γ" phase reduces by about 2%. When the strain rate is 0.1 s-1 and the deformation is 50%, the increase of deformation temperature can promote dynamic recrystallization and grain growth in the temperature range of 1070~1160 ℃. With the deformation temperature rising to 1130 ℃, a large quantity of γ" phase has dissolved, the ability to pin the grain boundary has been significantly weakened, and the average grain size has increased to 12.1 μm. At the deformation temperature of 1100 ℃, strain rate of 1 s-1 and deformation of 50%, fine and uniform “γ+γ′ dual-phase structure " and the grain size above ASTM 12 can be obtained.

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何英杰,馬向東,李遠,肖磊,楊金龍,郭建政,馮干江.變形參數(shù)對FGH4113A粉末高溫合金微觀組織演化的影響[J].稀有金屬材料與工程,2024,53(1):223~233.[heyingjie, maxiangdong, liyuan, xiaolei, yangjinglong, guojianzheng, fenganjiang. Effect of Deformation Parameters on Microstructure Evolution of FGH4113A Powder Metallurgy Superalloy[J]. Rare Metal Materials and Engineering,2024,53(1):223~233.]
DOI:10.12442/j. issn.1002-185X.20220969

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  • 收稿日期:2022-12-13
  • 最后修改日期:2023-02-16
  • 錄用日期:2023-03-07
  • 在線發(fā)布日期: 2024-01-29
  • 出版日期: 2024-01-24