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澆鑄制度對K4750合金室溫拉伸性能的影響
作者:
作者單位:

中國科學(xué)院金屬研究所 師昌緒先進材料創(chuàng)新中心 沈陽

作者簡介:

通訊作者:

中圖分類號:

TG244

基金項目:

中國博士后基金資助(項目號No. 2020M671403)


Influence of Casting Process on the Room Temperature Tensile Properties of Alloy K4750
Author:
Affiliation:

Shi -changxu Innovation Center for Advanced Materials,Institute of Metal Research,Chinese Academy of Sciences

Fund Project:

China Postdoctoral Science Foundation under Grant

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    摘要:

    K4750合金是一種新型鑄造鎳基高溫合金,在700-750℃具有較為優(yōu)異的力學(xué)性能,有望代替K4169合金使用。但是K4750合金的室溫拉伸塑性波動性較大,合金室溫拉伸性能、凝固組織和澆鑄制度之間的關(guān)系尚不明確。本工作采用不同的澆鑄溫度和型殼冷卻條件制備了多組K4750合金試棒,采用單軸拉伸測試了合金的室溫拉伸性能,評價了合金室溫拉伸性能對澆鑄溫度和型殼冷卻速率變化的敏感性,并通過組織表征進行了機理闡述。結(jié)果表明,澆鑄溫度降低,合金晶粒尺寸顯著減小,合金屈服強度小幅提高,塑性保持穩(wěn)定;而當型殼冷卻速率降低后,合金室溫拉伸斷后延伸率顯著下降。這主要是由于型殼冷卻條件顯著影響了MC碳化物的析出特征。當冷卻速率較低時,晶界析出粗大的長條狀MC碳化物,其在應(yīng)力作用下易于產(chǎn)生內(nèi)部裂紋,從而加速合金晶界失效降低合金塑性。為優(yōu)化K4750合金的室溫拉伸性能,應(yīng)重點關(guān)注型殼或鑄件在澆鑄后的冷卻速率與晶界MC碳化物析出形態(tài),抑制粗大晶界碳化物產(chǎn)生,提高晶界塑韌性。

    Abstract:

    K4750 alloy is a new cast nickel-based superalloy with excellent mechanical properties at 700-750℃ and is expected to replace K4169 alloy. However, the tensile plasticity of K4750 alloy at room temperature fluctuates, and the relationship among room temperature tensile properties, solidification microstructure, and casting parameters is still unclear for this alloy. In this work, several K4750 alloy test bars were prepared with various casting temperatures and shell cooling conditions, and tested at room temperature by uniaxial tension. Sensitivity of the alloy"s room temperature tensile properties to changes in casting temperature and shell cooling rate was evaluated, and the mechanism was elucidated by microstructure characterization. Results show that the grain size of alloy drops significantly with decreasing casting temperature, and the yield strength of alloy slightly increases while the plasticity remains stable. When cooling rate of the shell decreases, the fracture elongation of alloy decreases significantly at room temperature. This is mainly because the cooling condition of mold shell significantly affects the precipitation characteristics of MC carbides. When the cooling rate is low, MC carbides tend to precipitate at grain boundaries in coarse and strip-like shapes. MC carbides are prone to internal cracks under stress, accelerating the intergranular failure of material and reducing the plasticity of alloy. In order to optimize the tensile properties of K4750 alloy at room temperature, more attention should be paid to the cooling rate of mold shell after casting and the precipitation morphology of intergranular carbides, prohibiting the formation of coarse intergranular carbides to improve the grain boundary plasticity of alloy.

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引用本文

趙鵬飛,王旻,歐美瓊,馬穎澈,劉奎.澆鑄制度對K4750合金室溫拉伸性能的影響[J].稀有金屬材料與工程,2023,52(11):3809~3817.[Zhao Pengfei, Wang Min, Ou Mei Qiong, MA Yingche, Liu Qui. Influence of Casting Process on the Room Temperature Tensile Properties of Alloy K4750[J]. Rare Metal Materials and Engineering,2023,52(11):3809~3817.]
DOI:10.12442/j. issn.1002-185X.20220815

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  • 收稿日期:2022-10-18
  • 最后修改日期:2022-11-25
  • 錄用日期:2023-01-05
  • 在線發(fā)布日期: 2023-11-27
  • 出版日期: 2023-11-22