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熱處理及預(yù)拉伸對(duì)TC4-0.55Fe合金組織和力學(xué)性能的影響
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南京工業(yè)大學(xué)材料科學(xué)與工程學(xué)院/新材料研究院 南京 211816

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國(guó)家級(jí)大學(xué)生創(chuàng)新創(chuàng)業(yè)訓(xùn)練計(jì)劃項(xiàng)目成果(202110291008Z);國(guó)家重點(diǎn)研發(fā)計(jì)劃((No.2021YFB3700801));江蘇高校優(yōu)勢(shì)學(xué)科建設(shè)工程資助項(xiàng)目


Effect of Heat treatment and Pre-stretching on Microstructure and Mechanical Properties of TC4-0.55Fe Alloy
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College of Materials Science and Engineering and Tech Institute for Advanced Materials,Nanjing Tech University

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    摘要:

    本文研究了具有雙態(tài)組織的鈦合金Ti-6Al-4V-0.55Fe(TC4-0.55Fe)在不同熱處理制度(固溶時(shí)效、雙重退火)和引入預(yù)拉伸對(duì)微觀組織及力學(xué)性能的影響,并分析了合金顯微組織與力學(xué)性能之間的聯(lián)系。通過(guò)對(duì)雙態(tài)組織的 TC4-0.55Fe采用固溶時(shí)效和雙重退火熱處理后微觀組織和力學(xué)性能進(jìn)行比較,發(fā)現(xiàn)兩種熱處理方式下隨著時(shí)效和低溫退火溫度升高合金中微米級(jí)的片層α相厚度均逐漸增大、強(qiáng)度降低、塑性提高。固溶時(shí)效熱處理下隨著時(shí)效溫度的升高合金屈服強(qiáng)度從530℃的873MPa下降到590℃的862MPa,而延伸率提高3.2%。雙重退火熱處理試樣的屈服強(qiáng)度隨著低溫退火溫度的升高逐步降低,但是延伸率相比于固溶時(shí)效有了很大提高,最好可達(dá)到23.6%。由于普通熱處理對(duì)鈦合金強(qiáng)度提升不明顯,時(shí)效和低溫退火溫度均為590℃時(shí),雙重退火試樣塑性更優(yōu)于固溶時(shí)效,所以選擇該試樣引入預(yù)拉伸強(qiáng)化,對(duì)其在固溶和低溫退火中間進(jìn)行預(yù)拉伸。引入預(yù)拉伸后,晶粒發(fā)生了明顯的變形,進(jìn)行時(shí)效強(qiáng)化后合金組織無(wú)沉淀區(qū)(PFZ)中析出大量細(xì)小的二次α相(αs),引入預(yù)拉伸后進(jìn)行時(shí)效可以在提升鈦合金屈服強(qiáng)度的同時(shí)只降低極少的塑性,其中預(yù)拉伸形變1%的試樣等軸晶含量最高,強(qiáng)度較引入預(yù)拉伸前提高68MPa,延伸率僅下降4%,力學(xué)性能最優(yōu)。通過(guò)本文研究可知,TC4-0.55Fe鈦合金在經(jīng)過(guò)固溶處理后繼續(xù)進(jìn)行預(yù)拉伸和時(shí)效處理,可以有效提升合金的綜合力學(xué)性能。

    Abstract:

    This paper investigated the effects of different heat treatment processes (solution aging and double annealing) and pre-stretching on the microstructure and mechanical properties of Ti-6Al-4V-0.55Fe (TC4-0.55Fe) alloy with duplex microstructure and the relationship between microstructure and mechanical properties of TC4-0.55Fe alloy was analyzed. The microstructure and mechanical properties of the duplex microstructure after solution aging and double annealing were compared and it can be found that the thickness of the micron scale lamellar α phase gradually increased with the increase of aging and low temperature annealing temperature under the condition of two kinds of heat treatments, which reduced the strength and increased the plasticity of the alloy. Under the solution aging treatment, the yield strength of the samples decreases from 873MPa at 530℃ to 862MPa at 590℃ and the elongation increases by 3.2% with the increasing aging temperature. The yield strength of the double annealing heat treatment sample decreases gradually with the increase of the low temperature annealing temperature, but the elongation has been greatly improved compared with the solution aging, and the best is 23.6%.Because the strength of titanium alloy is not significantly improved by ordinary heat treatment, the plasticity of the double annealing sample is better than that of the solution aging when the aging and low temperature annealing temperature is 590 ℃, so the sample is selected to introduce the pre-stretching strengthening and pre-stretch it between the solution and low temperature annealing. After the introduction of pre-stretching, the grain deformation is obvious. And a large number of fine secondary α phase (αs) are precipitated in the precipitation-free zone (PFZ) of the alloy structure after aging strengthening. The aging after the introduction of pre-stretching can improve the yield strength of titanium alloy and only reduce a little plasticity. Among them, the sample with 1% pre-stretching deformation has the highest content of equiaxed grains, the strength is increased by 68MPa compared with that before the introduction of pre-stretching, and the elongation is only decreased by 4%, the mechanical properties are the best. According to this study, the comprehensive mechanical properties of TC4-0.55Fe titanium alloy can be improved by pre-stretching and aging strengthening after solution strengthening.

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劉思儂,張晶棋,劉博瑋,李鑫,李峰,常輝.熱處理及預(yù)拉伸對(duì)TC4-0.55Fe合金組織和力學(xué)性能的影響[J].稀有金屬材料與工程,2023,52(10):3485~3494.[Liu Sinong, Zhang Jingqi, Liu Bowei, Li Xin, Li Feng, Chang Hui. Effect of Heat treatment and Pre-stretching on Microstructure and Mechanical Properties of TC4-0.55Fe Alloy[J]. Rare Metal Materials and Engineering,2023,52(10):3485~3494.]
DOI:10.12442/j. issn.1002-185X.20220759

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  • 收稿日期:2022-09-25
  • 最后修改日期:2023-08-29
  • 錄用日期:2023-03-03
  • 在線發(fā)布日期: 2023-10-27
  • 出版日期: 2023-10-24