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含氮氣氛FSP表面改性純鈦的微結(jié)構(gòu)和織構(gòu)
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常熟理工學院 汽車工程學院

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江蘇省高等學校自然科學研究重大項目(項目號18KJA460001)


Microstructure and texture of pure titanium surface modificated by friction stir processing
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School of Automotive Engineering,Changshu Institute of Technology

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    本文研究了含氮氣氛下FSP表面改性純鈦的微結(jié)構(gòu)和織構(gòu)。結(jié)果表明:FSP純鈦攪拌區(qū)為等軸晶粒,靠近AS側(cè)和RS側(cè)的動態(tài)再結(jié)晶晶粒平均晶粒尺寸為2.29μm,近表面和中心區(qū)受溫升和摩擦攪拌的綜合作用,平均晶粒尺寸分別長大至6.48μm和8.64μm。FSP熱機影響區(qū)呈梯度分布,靠近攪拌區(qū)部分晶粒細化破碎嚴重;遠離攪拌區(qū)部分,原始晶粒變形小,以形變孿生機制為主。AS側(cè)、底部和RS側(cè)的熱機影響區(qū)寬度分別為900μm,700μm和480μm。熱機影響區(qū)內(nèi)主要形成{10-12}拉伸孿晶。攪拌針形狀是FSP純鈦微區(qū)織構(gòu)演變的重要影響因素,攪拌區(qū)晶粒的c軸接近于PD方向。受攪拌區(qū)晶粒細化和加工硬化共同作用,攪拌區(qū)硬度整體高于母材,硬度最大值達到223.7HV0.5

    Abstract:

    The microstructure and texture of FSP pure titanium in nitrogen atmosphere were investigated. The results showed that there were equiaxed grains in the stir zone. The average grain size of dynamic recrystallized grains near AS side and RS side was 2.29 μm. The combined effects of rising temperature and friction stir in the near surface and central zone, the average grain size grew to 6.48 μm and 8.64 μm respectively. The thermal-mechanical affect zone presented a gradient distribution. The grains near the stir zone had been seriously broken and refined. In the zone far away from the stir zone, the deformation of the original grains was slightly, and the deformation mechanism was dominated by deformation twinning. The width of the thermal-mechanical affect zone at AS side, bottom and RS side was 900 μm,700 μm and 480 μm respectively. The mainly deformation twins in the thermal-mechanical affect zone were {10-12} tensile twins. The structure of stirring pin was an important factor affecting the texture evolution of FSP pure titanium. Moreover, the c-axises of the grains in the stir zone were distributed close to the PD direction. Due to the combined effect of grain refinement and work hardening, the hardnesses in the stir zone were overall higher than the initial material, and the maximum hardness reached to 223.7HV0.5.

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許峰,林芷民,繆茹萍,譚珊.含氮氣氛FSP表面改性純鈦的微結(jié)構(gòu)和織構(gòu)[J].稀有金屬材料與工程,2023,52(9):3206~3212.[Xu Feng, Lin Zhimin, Miao Ruping, Tan Shan. Microstructure and texture of pure titanium surface modificated by friction stir processing[J]. Rare Metal Materials and Engineering,2023,52(9):3206~3212.]
DOI:10.12442/j. issn.1002-185X.20220738

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  • 收稿日期:2022-09-16
  • 最后修改日期:2022-10-31
  • 錄用日期:2022-11-10
  • 在線發(fā)布日期: 2023-09-25
  • 出版日期: 2023-09-21