2相"/> 2相尺寸更細小,密度更高,且多為半共格的η′相,位錯塞積演變?yōu)閬喚?二者交互作用更強,起到更好的強化效果。最優(yōu)熱處理制度為單級固溶+單級時效,在此條件下,抗拉強度與延伸率分別達到747MPa和4.3%,優(yōu)于雙級固溶+雙級時效制度。"/>

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基于往復擠壓的7034鋁合金形變熱處理強韌化機理研究
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合肥工業(yè)大學 材料科學與工程學院 高性能銅合金材料及成形加工教育部工程研究中心

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國家自然科學基金資助項目(51975175,51875158,52005145)


Study on the Strengthening and Toughening Mechanisms of 7034 Aluminum Alloy Subjected to Reciprocating Extrusion Based Thermo-Mechanical Treatment
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School of Materials Science and Engineering,Hefei University of Technology,Hefei 23009,China

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    摘要:

    為提高7034鋁合金微觀組織均勻性和綜合力學性能,本文開展了往復擠壓劇烈塑性變形工藝與固溶時效制度的優(yōu)化設計研究,并表征了不同變形-熱處理方案下材料力學性能、晶粒與第二相尺寸分布、位錯組態(tài)演化的定量規(guī)律,建立了塑性變形和熱處理制度與7034鋁合金的微觀組織和力學性能的關(guān)聯(lián)關(guān)系。結(jié)果表明:經(jīng)過三道次往復擠壓,平均晶粒尺寸由初始態(tài)的59μm細化到9μm,平均晶粒尺寸標準差從一道次的3.05下降到三道次的0.8;相較于雙級固溶時效,單級固溶時效處理后的MgZn2相尺寸更細小,密度更高,且多為半共格的η′相,位錯塞積演變?yōu)閬喚?二者交互作用更強,起到更好的強化效果。最優(yōu)熱處理制度為單級固溶+單級時效,在此條件下,抗拉強度與延伸率分別達到747MPa和4.3%,優(yōu)于雙級固溶+雙級時效制度。

    Abstract:

    In order to improve the uniformity of microstructure and comprehensive mechanical properties of 7034 aluminum alloy, this paper carried out the optimization design of the severe plastic deformation process and solution and aging treatment based on the reciprocating extrusion, characterized the mechanical properties of the material, the size distribution of grain and secondary phase and the quantification of dislocation configuration evolution, established the relationship between plastic deformation and heat treatment and the microstructure and mechanical properties of 7034 aluminum alloy. The results show that, the average grain size is refined from 59μm to 9μm, and the standard deviation of the average grain size decreases from 3.05 to 0.8 after three passes reciprocating extrusion; Compared with the two-stage solution and aging treatment, the MgZn2 phase after single-stage solution and aging treatment is smaller in size, higher in density, and mostly semi-coherent η" phase, and the dislocations pile-up becomes in sub-grain. The interaction between the two is stronger and the strengthening effect is better. The optimal heat treatment system is single-stage solution + single-stage aging. under this condition, the tensile strength and elongation reach 747MPa and 4.3% respectively, which are better than the two-stage solution + two-stage aging system.

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薛克敏,張峻源,嚴思梁,許 兵,李 萍.基于往復擠壓的7034鋁合金形變熱處理強韌化機理研究[J].稀有金屬材料與工程,2023,52(9):3089~3096.[XUE Ke-min, ZHANG Jun-yuan, YAN Si-liang, XU Bing, LI Ping. Study on the Strengthening and Toughening Mechanisms of 7034 Aluminum Alloy Subjected to Reciprocating Extrusion Based Thermo-Mechanical Treatment[J]. Rare Metal Materials and Engineering,2023,52(9):3089~3096.]
DOI:10.12442/j. issn.1002-185X.20220680

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  • 收稿日期:2022-08-31
  • 最后修改日期:2022-11-23
  • 錄用日期:2022-11-25
  • 在線發(fā)布日期: 2023-09-25
  • 出版日期: 2023-09-21