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時效+再結(jié)晶退火對鎳基合金鍛造混晶組織的影響
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1.三門核電有限公司;2.中南大學(xué) 機電工程學(xué)院;3.浙江浙能技術(shù)研究院有限公司 材料技術(shù)所

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TG132.2

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國家自然科學(xué)基金(編號:51775564),湖南省科技人才托舉工程(2020TJ-Q05)


Effect of the aging and recrystallization annealing treatment on the forged mixed grain structure of Ni-based superalloy
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    摘要:

    為了消減鎳基合金鍛件中的混晶組織,本文提出了δ相時效+再結(jié)晶退火的熱處理工藝路線。δ相在時效過程中可以直接析出或者由γ″相發(fā)生相變間接析出。對含析出δ相的材料進行高溫再結(jié)晶退火,然后立即水冷,可以發(fā)現(xiàn)時效方式和時效時間對退火過程中的組織演變存在顯著影響。時效過程中直接析出的δ相主要分布在晶界,隨著時效時間延長部分晶粒內(nèi)部也會析出δ相,其形貌以短棒狀為主。間接析出的δ相主要分布在晶粒內(nèi)部以及晶界,其形貌主要為晶內(nèi)長針狀以及晶界短棒狀。短棒狀δ相在退火過程中與位錯交互作用較弱,主要起到釘扎晶界的作用;而長針狀δ相能夠促使亞晶的形成。因此,間接時效方式有利于再結(jié)晶形核的發(fā)生,并能夠有效阻礙晶粒生長避免異常長大的再結(jié)晶晶粒。

    Abstract:

    In order to eliminate the mixed grain structure of forged Ni-based superalloy parts, the heat treatment process of δ phase aging + recrystallization annealing was proposed. During aging, the δ phase can precipitate directly or indirectly by the transformation of γ″ phase. The alloy with precipitated δ phases were both annealed at high temperature and then immediately cooled by water. It was found that the aging routes and aging times greatly affect the microstructure evolution during recrystallization annealing. In the aging process, the directly-precipitated δ phase mainly distributes at grain boundaries. With the increase of aging time, some δ phases precipitate inside grains, and the main morphology is short-rod like. The distribution characteristic of the indirectly-precipitated δ phase is mainly intragranular needle like and intergranular short-rod like. The short-rod δ phase has weak interaction with dislocations during annealing and is mainly responsible for pinning grain boundaries, while the long needle-like δ phase can promote the formation of sub-grains. That is why the indirect aging is favorable for the recrystallization nucleation, and can also effectively hinder the growth of grains to avoid abnormal growth of recrystallized grains.

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楊志明,陳子健,藺永誠,樓玉民,黃一君.時效+再結(jié)晶退火對鎳基合金鍛造混晶組織的影響[J].稀有金屬材料與工程,2023,52(9):3147~3152.[Yang zhiming, Chen zijian, lin yongcheng, lou yumin, huang yijun. Effect of the aging and recrystallization annealing treatment on the forged mixed grain structure of Ni-based superalloy[J]. Rare Metal Materials and Engineering,2023,52(9):3147~3152.]
DOI:10.12442/j. issn.1002-185X.20220676

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歷史
  • 收稿日期:2022-08-30
  • 最后修改日期:2022-11-19
  • 錄用日期:2022-11-24
  • 在線發(fā)布日期: 2023-09-25
  • 出版日期: 2023-09-21