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FGH113A (WZ-A3) 粉末高溫合金長期組織穩(wěn)定性研究
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作者單位:

1.中南大學(xué) 粉末冶金國家重點(diǎn)實(shí)驗(yàn)室;2.深圳市萬澤中南研究院有限公司

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基金項(xiàng)目:

國家科技重大專項(xiàng)( 2017-Ⅵ-0009-0080 )


Study on Microstructure Long-term Stability of Powder Metallurgy Superalloy FGH113A(WZ-A3)
Author:
Affiliation:

1.State Key Laboratory of Powder Metallurgy,Central South University;2.Shenzhen Wedge Central South Research Institute Co,Ltd

Fund Project:

National Science and Technology Major Project(2017-Ⅵ-0009-0080)

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    摘要:

    采用光學(xué)顯微鏡、掃描電鏡及能譜儀等觀察分析了760℃和815℃長期時(shí)效下,FGH113A(WZ-A3)合金的晶粒組織、γ′強(qiáng)化相、碳化物等演變規(guī)律,通過力學(xué)性能測試分析了長期時(shí)效對合金拉伸性能的影響。結(jié)果表明:760℃和815℃長期時(shí)效對合金的晶粒尺寸與形貌均無明顯影響。760℃長期時(shí)效后合金的γ′強(qiáng)化相尺寸與形貌無明顯變化,但815℃長期時(shí)效至440h,γ′相開始長大且形貌由近立方狀向近球形轉(zhuǎn)化。760℃長期時(shí)效2020h后,碳化物由彌散分布的顆粒狀,轉(zhuǎn)變?yōu)榫Ы缇奂龀鲞B續(xù)型碳化物;815℃長期時(shí)效440h后,晶內(nèi)開始析出針狀碳化物,2020h后明顯可見顆粒狀碳化物在晶界富集,晶內(nèi)針狀碳化物持續(xù)增多。在704℃和760℃拉伸測試條件下,長期時(shí)效760℃/440h和760℃/2020h合金抗拉強(qiáng)度相當(dāng),屈服強(qiáng)度在2020h后反而有小幅提升;長期時(shí)效815℃下,合金拉伸性能表現(xiàn)出類似規(guī)律,拉伸強(qiáng)度較好與晶粒度保持穩(wěn)定和晶界碳化物的釘扎作用有關(guān)。新型鎳基粉末高溫合金FGH113A在760℃和815℃長期時(shí)效下表現(xiàn)出優(yōu)異的穩(wěn)定性。

    Abstract:

    The evolution of grain structures, γ" strengthening phases and carbides of FGH113A (WZ-A3) alloy during long-term aging treatment at 760 ℃ and 815 ℃ were studied by means of Optical Microscope (OM), Scanning Electron Microscope (SEM), and Energy Dispersive Spectrometer (EDS) and the effect of long-term aging on the tensile properties of the alloy was analyzed. The results show that the long-term aging at 760℃ and 815℃ has no significant effect on grain size and grain morphology of the alloy. After long-term aging at 760℃, the size and morphology of the γ" strengthening phases have no obvious effect, but after long-term aging at 815℃ for 440h, the γ" phases begin to grow and the morphology changes from quasi-cubic to quasi-spherical. After long-term aging at 760℃ for 2020h, the carbides have changed from dispersed granular particles to aggregated at grain boundaries. After long-term aging at 815℃ for 440h, needle-like carbides begin to precipitate in the grains. After 2020h, granular carbides are enriched at the grain boundaries and form chains, at the same time, the needle-like carbides precipitated in the grains further increased. Under the tensile tests of 704°C and 760°C, the tensile strengths of the alloy during long-term aging treatment 760°C/440h and 760°C/2020h were equivalent, but the yield strengths increased slightly after 2020h; the tensile properties of the alloy show similar discipline at 815 long-term aging. The key reasons for the better tensile strength stability of the alloy were attributed to the stable grain structures and the pinning effect of grain boundary carbides. The new nickel-based powder superalloy FGH113A exhibits excellent stability under long-term aging at 760°C and 815°C.

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引用本文

熊江英,尹超,王沖,郭建政. FGH113A (WZ-A3) 粉末高溫合金長期組織穩(wěn)定性研究[J].稀有金屬材料與工程,2023,52(8):2885~2892.[Xiong Jiangying, Yin Chao, Wang Chong, Guo Jiangzheng. Study on Microstructure Long-term Stability of Powder Metallurgy Superalloy FGH113A(WZ-A3)[J]. Rare Metal Materials and Engineering,2023,52(8):2885~2892.]
DOI:10.12442/j. issn.1002-185X.20220656

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  • 收稿日期:2022-08-17
  • 最后修改日期:2022-10-26
  • 錄用日期:2022-11-09
  • 在線發(fā)布日期: 2023-08-28
  • 出版日期: 2023-08-24