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熱處理對(duì)一種抗熱腐蝕單晶高溫合金組織和持久性能的影響
作者:
作者單位:

1.中國(guó)科學(xué)院金屬研究所;2.遼寧科技大學(xué)機(jī)械工程與自動(dòng)化學(xué)院

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中圖分類號(hào):

TG146.1+5

基金項(xiàng)目:

國(guó)家重點(diǎn)研發(fā)計(jì)劃(2021YFC2202402);遼寧省科技攻關(guān)計(jì)劃課題(2019JH2/10100009)


Effect of Heat Treatment on Microstructures and Stress Rupture Properties of a Hot-Corrosion Resistant Single Crystal Superalloy
Author:
Affiliation:

1.Institute of Metal Research, Chinese Academy of Sciences;2.School of Mechanical Engineering and Automation, University of Science and Technology Liaoning

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    摘要:

    研究了熱處理對(duì)一種抗熱腐蝕單晶高溫合金微觀組織及1070 ℃/140 MPa持久性能的影響。結(jié)果表明:長(zhǎng)時(shí)間的均勻化熱處理顯著降低了元素偏析;隨著均勻化時(shí)間的延長(zhǎng),微孔面積分?jǐn)?shù)逐漸增加,平均尺寸不斷增大,微孔的密度呈先升高后降低的變化趨勢(shì);隨一級(jí)時(shí)效溫度的升高,γ′相尺寸逐漸增大,γ′相面積分?jǐn)?shù)先增加后減少;合金的持久壽命隨一級(jí)時(shí)效溫度的提高先升高后降低,一級(jí)時(shí)效溫度為1100 ℃時(shí),立方狀γ′相尺寸約370 nm且正方度較好,γ′相的面積分?jǐn)?shù)最大,持久壽命最高;持久斷口具有韌性斷裂特征,亞晶界處的碳化物和微孔是引起持久試樣斷裂的主要裂紋源。

    Abstract:

    The effects of heat treatment on the microstructures and rupture properties at 1070 ℃/140 MPa of a hot-corrosion resistant single crystal superalloy was investigated. The results show that long-term homogenization heat treatment significantly reduces element segregation. With the extension of homogenization time, the area fraction of micropores gradually increases, the average size keeps increasing, and the density of micropores increases firstly and then decreases. With the increase of primary aging temperature, the size of γ" phase enlarge gradually, the area fraction of γ" phase frist increases and then decreases. The stress rupture life of the alloy increases first and then decreases with the increase of the primary aging temperature. When the primary aging temperature is 1100 ℃, the size of the cubic γ" phase is about 370 nm and the squareness is better, the area fraction of the γ" phase is the largest and the stress rupture life is the highest. The stress rupture fracture is characterized by ductile fracture. The carbides and micropores at the sub-grain boundary are the main crack sources that cause the stress rupture fracture of the sample.

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來(lái)永軍,寧禮奎,柳一川,劉恩澤,孟祥倫,譚政,佟健,鄭志.熱處理對(duì)一種抗熱腐蝕單晶高溫合金組織和持久性能的影響[J].稀有金屬材料與工程,2023,52(6):2243~2252.[laiyongjun, ninglikui, liuyichuan, liuenze, mengxianglun, tanzheng, tongjian, zhengzhi. Effect of Heat Treatment on Microstructures and Stress Rupture Properties of a Hot-Corrosion Resistant Single Crystal Superalloy[J]. Rare Metal Materials and Engineering,2023,52(6):2243~2252.]
DOI:10.12442/j. issn.1002-185X.20220589

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  • 收稿日期:2022-07-15
  • 最后修改日期:2022-10-25
  • 錄用日期:2022-11-09
  • 在線發(fā)布日期: 2023-07-07
  • 出版日期: 2023-06-30