-1的條件下,對(duì)置氫TC17鈦合金進(jìn)行了高溫壓縮實(shí)驗(yàn),研究了置氫TC17鈦合金的熱變形行為,并對(duì)其熱變形激活能進(jìn)行了計(jì)算分析。結(jié)果顯示,TC17鈦合金原始組織為典型的網(wǎng)籃組織,由α+β相組成,隨著氫含量的增加,針狀α相數(shù)量減少,β相增多,當(dāng)氫含量超過0.40wt%時(shí),鈦合金中依次出現(xiàn)了γ氫化物和δ氫化物。置氫TC17鈦合金不僅是溫度敏感型材料、速率敏感型材料,也是氫含量敏感型材料,在氫含量0.2wt%時(shí),峰值應(yīng)力達(dá)到最小值,與原始合金相比,變形溫度可降低40℃,應(yīng)變速率可提高1個(gè)數(shù)量級(jí)。同時(shí),氫含量0.2wt%的TC17鈦合金變形激活能也達(dá)到最小值162KJ/mol,其熱變形軟化機(jī)制為動(dòng)態(tài)回復(fù)。"/>

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置氫TC17鈦合金組織演變規(guī)律及高溫變形行為
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1.北京科技大學(xué) 材料科學(xué)與工程學(xué)院;2.中國航空制造技術(shù)研究院

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國家自然科學(xué)基金資助(項(xiàng)目號(hào)52075509)


Microstructure Evolution and Deformation Behavior of Hydrogenated TC17 titanium alloy
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1.Material science and Engineering School,University of Science and Technology Beijing;2.AVIC Manufacturing Technology Institute

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    摘要:

    為了改善了TC17鈦合金熱加工性能,對(duì)TC17鈦合金進(jìn)行了置氫處理,通過金相觀察和X射線衍射分析,研究了置氫后TC17鈦合金的微觀組織及相轉(zhuǎn)變規(guī)律,在變形溫度800 ~ 860℃、應(yīng)變速率0.001 ~ 0.1s-1的條件下,對(duì)置氫TC17鈦合金進(jìn)行了高溫壓縮實(shí)驗(yàn),研究了置氫TC17鈦合金的熱變形行為,并對(duì)其熱變形激活能進(jìn)行了計(jì)算分析。結(jié)果顯示,TC17鈦合金原始組織為典型的網(wǎng)籃組織,由α+β相組成,隨著氫含量的增加,針狀α相數(shù)量減少,β相增多,當(dāng)氫含量超過0.40wt%時(shí),鈦合金中依次出現(xiàn)了γ氫化物和δ氫化物。置氫TC17鈦合金不僅是溫度敏感型材料、速率敏感型材料,也是氫含量敏感型材料,在氫含量0.2wt%時(shí),峰值應(yīng)力達(dá)到最小值,與原始合金相比,變形溫度可降低40℃,應(yīng)變速率可提高1個(gè)數(shù)量級(jí)。同時(shí),氫含量0.2wt%的TC17鈦合金變形激活能也達(dá)到最小值162KJ/mol,其熱變形軟化機(jī)制為動(dòng)態(tài)回復(fù)。

    Abstract:

    In order to improve the hot workability of TC17 titanium alloy, TC17 titanium alloy was hydrogenated. Through metallographic observation and X-ray diffraction analysis, the microstructure and phase transformation law of TC17 titanium alloy were studied after hydrogenated treatment. Under the conditions of deformation temperature of 800-860℃ and strain rate of 0.001-0.1s-1, the isothermal compression tests of hydrogenated TC17 titanium alloy were carried out. The deformation behavior of the hydrogenated TC17 titanium alloy was studied, and the thermal activation energy was calculated and analyzed. The results show that the microstructure of TC17 titanium alloy is a typical net basket structure, which is composed of α+β phase composition. With the increasing of hydrogen content, the volume fraction of acicular α phase decreases, and the volume fraction of β phase increases. When the hydrogen content exceeds 0.40wt%, the γ and δ hydrides separate out. The hydrogenated TC17 titanium alloy is not only a temperature sensitive material, a rate sensitive material, but also a hydrogen content sensitive material. When the hydrogen content is 0.2wt%, the peak stress reaches the minimum value. Compared with the original alloy, the deformation temperature can be deincreased by 40℃ and the strain rate can be increased by one order of magnitude. At the same time, the thermal activation energy of TC17 titanium alloy with 0.2wt% hydrogen content also reaches the minimum value of 162KJ/mol, and its thermal deformation softening mechanism was dynamic recovery.

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周昊,王耀奇,李紅,任學(xué)平,侯紅亮.置氫TC17鈦合金組織演變規(guī)律及高溫變形行為[J].稀有金屬材料與工程,2023,52(3):947~952.[Zhou Hao, Wang Yaoqi, Li Hong, Ren Xueping, Hou HongLiang. Microstructure Evolution and Deformation Behavior of Hydrogenated TC17 titanium alloy[J]. Rare Metal Materials and Engineering,2023,52(3):947~952.]
DOI:10.12442/j. issn.1002-185X.20220509

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  • 收稿日期:2022-06-11
  • 最后修改日期:2022-09-07
  • 錄用日期:2022-09-19
  • 在線發(fā)布日期: 2023-04-07
  • 出版日期: 2023-03-24