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退火對(duì)液氮軋制CrCoNi中熵合金組織與性能的影響
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昆明理工大學(xué)材料科學(xué)與工程學(xué)院

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TG337

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云南省科技廳面向基金(項(xiàng)目號(hào)908075156031),釩鈦資源綜合利用四川省重點(diǎn)實(shí)驗(yàn)室項(xiàng)目(2021FTSZ13),攀枝花學(xué)院校級(jí)項(xiàng)目(2021YB009)。通信作者易健宏(1965—),男,湖南長沙人,博士,教授,主要從事稀貴金屬材料加工與制備研究,E-mail:yijianhong@kmust.edu.cn


Effect of annealing on microstructure and properties of medium entropy alloy CrCoNi after liquid nitrogen temperature rolling
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    摘要:

    針對(duì) CrCoNi中熵合金具有優(yōu)異的液氮性能,但其液氮軋制后塑性較差(<8%)所帶來的難加工問題,本文以電弧熔煉鑄態(tài)CrCoNi中熵合金為研究對(duì)象,在液氮(77K)下對(duì)CrCoNi合金進(jìn)行了3道次軋制變形,總變形量為50 %。隨后,采用650 ℃、700 ℃、800 ℃三種溫度,保溫時(shí)間為30 min下進(jìn)行退火。實(shí)驗(yàn)數(shù)據(jù)表明:CrCoNi中熵合金經(jīng)過軋制及退火后,未發(fā)生物相結(jié)構(gòu)改變,退火后,變形晶粒發(fā)生再結(jié)晶細(xì)化,并產(chǎn)生∑3退火孿晶,隨退火溫度升高,再結(jié)晶程度增加,延伸率提高,通過液氮軋制與中溫短時(shí)間退火進(jìn)行性能調(diào)控,可獲得強(qiáng)度與韌性匹配的性能,并提高了熱處理工藝效率。

    Abstract:

    The medium entropy alloy of CrCoNi has excellent low temperature properties, but its plasticity is poor (<8%) after liquid nitrogen temperature rolling. In this research, arc melting of casted CrCoNi entropy alloy as the research sample, rolling deformation of CrCoNi alloy at low temperature (77K) for three passes, the total deformation was 50%. Then, annealing was carried out at 650 ℃, 700 ℃ and 800 ℃ for 30 minutes. Experimental data show that: CrCoNi medium entropy alloy after rolling and annealing, not material phase structure changed, after annealing. Because of recrystallization, deformation grains become smaller, and generated ∑3 annealing twin in organization. As the annealing temperature increased, the number of recrystallized grains increased, the elongation increased. It can be concluded that through the cold rolling and medium temperature annealing in short time performance controlling, matching the performance of the strength and toughness can be obtained, The efficiency of heat treatment process was improved.

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陳今良,馮中學(xué),易健宏.退火對(duì)液氮軋制CrCoNi中熵合金組織與性能的影響[J].稀有金屬材料與工程,2023,52(6):2182~2188.[chenjinliang, feng zhongxue, Yi jianhong. Effect of annealing on microstructure and properties of medium entropy alloy CrCoNi after liquid nitrogen temperature rolling[J]. Rare Metal Materials and Engineering,2023,52(6):2182~2188.]
DOI:10.12442/j. issn.1002-185X.20220473

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  • 收稿日期:2022-05-30
  • 最后修改日期:2022-06-17
  • 錄用日期:2022-07-12
  • 在線發(fā)布日期: 2023-07-07
  • 出版日期: 2023-06-30