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TiC增強(qiáng)FeMnCu中熵合金基復(fù)合材料的制備及其力學(xué)性能
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南京理工大學(xué) 材料科學(xué)與工程學(xué)院,江蘇 南京 210094

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National Natural Science Foundation of China (No. 51571118)


Preparation and Mechanical Properties of FeMnCu Medium Entropy Alloy Matrix Composites Reinforced with TiC Particles
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College of Materials Science and Engineering, Nanjing University of Science and Technology, Nanjing 210094, China

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National Natural Science Foundation of China (51571118)

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    摘要:

    采用真空感應(yīng)熔煉法制備xTiC/FeMnCu(x=2.5,5,7.5,10,vol%)復(fù)合材料,并對(duì)其進(jìn)行退火熱處理。采用X射線衍射儀(XRD)、掃描電鏡(SEM)、萬(wàn)能試驗(yàn)機(jī)等對(duì)所制備合金試樣的晶體結(jié)構(gòu)、成分、形貌、力學(xué)性能等進(jìn)行分析。結(jié)果表明,xTiC/FeMnCu復(fù)合材料呈現(xiàn)出雙相面心立方(fcc)結(jié)構(gòu)。隨著TiC含量的增加,復(fù)合材料的基體組織得到明顯細(xì)化,抗拉強(qiáng)度逐漸增大,這可能是細(xì)晶強(qiáng)化、熱錯(cuò)配強(qiáng)化、Orowan強(qiáng)化共同作用的結(jié)果。10TiC/FeMnCu經(jīng)600 ℃/4 h、800 ℃/4 h退火后,結(jié)構(gòu)沒(méi)有明顯變化,基體中有碳化物析出,試樣的抗拉強(qiáng)度小幅提升但延伸率略有降低。

    Abstract:

    xTiC/FeMnCu(x=2.5, 5, 7.5, 10, vol%) composites were fabricated by vacuum induction melting and then annealed. X-ray diffraction (XRD), scanning electron microscope (SEM) and energy dispersive spectrum (EDS) were used to analyze the phase constitution and microstructure, and the tensile properties of the samples were investigated by the universal tensile testing machine. The results show that the xTiC/FeMnCu(x=2.5, 5, 7.5, 10, vol%) composites exhibit a biphasic face-centred cubic structure. With the increase in x value, the matrix structure of the composites is significantly refined and the tensile strength gradually increases, which is due to the combined effect of fine grain strengthening, thermal mismatch strengthening and Orowan strengthening. After 10TiC/FeMnCu is annealed at 600 °C for 4 h and 800 °C for 4 h, the structure does not change significantly, and carbides are precipitated in the matrix. The tensile strength of the sample increases but the elongation decreases slightly.

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引用本文

李嘉雯,劉思聰,黃思睿,朱和國(guó).TiC增強(qiáng)FeMnCu中熵合金基復(fù)合材料的制備及其力學(xué)性能[J].稀有金屬材料與工程,2023,52(4):1169~1175.[Li Jiawen, Liu Sicong, Huang Sirui, Zhu Heguo. Preparation and Mechanical Properties of FeMnCu Medium Entropy Alloy Matrix Composites Reinforced with TiC Particles[J]. Rare Metal Materials and Engineering,2023,52(4):1169~1175.]
DOI:10.12442/j. issn.1002-185X.20220378

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  • 收稿日期:2022-05-02
  • 最后修改日期:2022-07-31
  • 錄用日期:2022-08-11
  • 在線發(fā)布日期: 2023-04-28
  • 出版日期: 2023-04-25