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電熔剛玉對硅基陶瓷型芯性能的影響
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上海大學省部共建高品質(zhì)特殊鋼冶金與制備國家重點實驗室

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國家自然科學基金項目(項目號92060104),國家科技重大專項(項目號2017- VII-0008-0102),上海市科委項目(項目號20511107700)中國重燃項目(F095)


Effect of fused corundum on properties of silicon-based ceramic core
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National Natural Science Foundation of China (Project No. 92060104), National Science and Technology Major Project (Project No. 2017-VII-0008-0102), Shanghai Science and Technology Commission Project (Project No. 20511107700),China United Gas Turbine Technology Project(F095))

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    摘要:

    以石英玻璃粉為原料,石蠟為增塑劑,添加0%~30%的電熔剛玉為礦化劑,通過熱壓注法成功制備了硅基陶瓷型芯,研究了電熔剛玉含量對方石英析晶和硅基陶瓷型芯綜合性能的影響。結果表明:隨著電熔剛玉含量的增加,樣品的收縮率逐漸增加,氣孔率先減小后增大,致密化程度增加;而抗彎強度和高溫抗蠕變性能呈現(xiàn)先增強后減弱的趨勢。當添加10%電熔剛玉時,樣品表現(xiàn)出優(yōu)良的綜合性能,收縮率為1.02%,氣孔率為20.91%,體積密度為1.7083g·cm3,室溫和高溫抗彎強度分別為14.83MPa和20.96 MPa,高溫撓度為0.39mm。

    Abstract:

    In order to study the effect of fused corundum content on properties of silicon-based ceramic cores, the ceramic cores with different amount of fused corundum(0%~30%) were prepared by the hot injection method, where quartz glass powder was used as raw materials, fused corundum as mineralizer, and the ceramic casting wax as the plasticizer. The results showed that with the increase of fused corundum, the shrinkage of the samples increased gradually, the porosity decreased at first and then increased, resulting in the higher degree of densification, while the flexural strength and high temperature creep resistance were falling after firstly climbing. When 10% fused corundum was added, the sample showed excellent comprehensive properties, with a shrinkage of 1.02%, a porosity of 20.91%, a bulk density of 1.7083 g·cm3, a bending strength of 14.83MPa and 20.96 MPa at room temperature and high temperature, and a high temperature deflection of 0.39 mm.

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周宇豪,玄偉東,任興孚,任忠鳴.電熔剛玉對硅基陶瓷型芯性能的影響[J].稀有金屬材料與工程,2023,52(4):1396~1402.[Zhouyuhao, Xuanweidong, Renxingfu, Renzhongming. Effect of fused corundum on properties of silicon-based ceramic core[J]. Rare Metal Materials and Engineering,2023,52(4):1396~1402.]
DOI:10.12442/j. issn.1002-185X.20220267

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  • 收稿日期:2022-03-31
  • 最后修改日期:2022-05-09
  • 錄用日期:2022-05-25
  • 在線發(fā)布日期: 2023-05-01
  • 出版日期: 2023-04-25