中間b路徑>外側(cè)c路徑;采用這種一模雙孔的擠壓方式,可以使進(jìn)料口中心粗大的Al4Sr相粒子經(jīng)過(guò)等通道模具中應(yīng)變最大的a路徑,使其得到有效細(xì)化,最終使得產(chǎn)品中心和邊緣的Al4Sr相均得到有效細(xì)化,尺寸約為4.5 μm。透射電鏡觀察表明,經(jīng)過(guò)大塑性變形后,由于累積應(yīng)變值增加,微觀應(yīng)變?cè)龃?,Al4Sr相內(nèi)部位錯(cuò)纏結(jié)交割,形成位錯(cuò)墻,與外部位錯(cuò)相互作用,使Al4Sr相粒子斷裂碎化,對(duì)Al4Sr相粒子產(chǎn)生了顯著的細(xì)化效果,同時(shí)由于界面能的增大,促使Al4Sr相出現(xiàn)少量回溶。"/>

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大應(yīng)變條件下鋁鍶合金連續(xù)擠壓組織演變
作者:
作者單位:

1.大連交通大學(xué);2.大連康豐科技有限公司

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基金項(xiàng)目:

國(guó)家自然科學(xué)基金資助項(xiàng)目(51705062);遼寧省科技攻關(guān)計(jì)劃項(xiàng)目(2021JH1/10400080)


Microstructure evolution of aluminum–strontium alloy continuous extrusion under large strain
Author:
Affiliation:

Dalian Jiaotong University

Fund Project:

National Natural Science Foundation of China(51705062);Liaoning Province Science and Technology Research Project (2021JH1/10400080)

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    摘要:

    摘要:本研究將連續(xù)擠壓與等通道模具相結(jié)合,通過(guò)有限元模擬、金相顯微鏡、X射線衍射儀和透射電子顯微鏡分析大應(yīng)變條件下鋁鍶中間合金微觀組織的變化機(jī)理。結(jié)果表明:等通道模具中等效應(yīng)變最大值可達(dá)16,出現(xiàn)在經(jīng)過(guò)第一轉(zhuǎn)角外角的a路徑上,對(duì)Al4Sr相細(xì)化效果最好,各路徑對(duì)Al4Sr相的細(xì)化作用為:內(nèi)側(cè)a路徑>中間b路徑>外側(cè)c路徑;采用這種一模雙孔的擠壓方式,可以使進(jìn)料口中心粗大的Al4Sr相粒子經(jīng)過(guò)等通道模具中應(yīng)變最大的a路徑,使其得到有效細(xì)化,最終使得產(chǎn)品中心和邊緣的Al4Sr相均得到有效細(xì)化,尺寸約為4.5 μm。透射電鏡觀察表明,經(jīng)過(guò)大塑性變形后,由于累積應(yīng)變值增加,微觀應(yīng)變?cè)龃?,Al4Sr相內(nèi)部位錯(cuò)纏結(jié)交割,形成位錯(cuò)墻,與外部位錯(cuò)相互作用,使Al4Sr相粒子斷裂碎化,對(duì)Al4Sr相粒子產(chǎn)生了顯著的細(xì)化效果,同時(shí)由于界面能的增大,促使Al4Sr相出現(xiàn)少量回溶。

    Abstract:

    Abstract: In this study, the continuous extrusion is combined with an equal-channel die. The microstructure evolution of Al-Sr master alloy under large strain extrusion is analyzed by finite-element simulation, metallographic microscopy, X-ray diffraction, and transmission electron microscopy. Results show that the maximum effective strain in the equal-channel die can reach 16, which appears on the a-path passing through the outer corner of the first die angle, and the refinement effect of Al4Sr phase is the best. The refinement effect of each path on Al4Sr phase is as follows: inner a-path > middle b- path > outside c-path. Using the extrusion method with one die of double hole, the coarse Al4Sr phase particles in the center of cavity inlet can pass through the a-path with largest strain in the equal-channel die, so that they can be effectively refined. Finally the particles of Al4Sr phase in the center and edge of the product are effectively refined, with an average length of about 4.5 μm. Transmission electron microscopy observation shows that after large plastic deformation, due to the increased cumulative strain and increased microscopic strain, the internal dislocations of Al4Sr phase are entangled and delivered, forming a dislocation wall that interacts with the external dislocations to break Al4Sr phase particles. The fragmentation exerts a significant refining effect on Al4Sr phase particles. At the same time, due to the increased interfacial energy, a small amount of Al4Sr phase dissolves.

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趙穎,王俊霖,運(yùn)新兵,郭麗麗,閆志勇,張旭.大應(yīng)變條件下鋁鍶合金連續(xù)擠壓組織演變[J].稀有金屬材料與工程,2023,52(3):1094~1102.[Zhao Ying, Wang Junlin, Yun Xinbing, Guo Lili, Yan Zhiyong, Zhang Xu. Microstructure evolution of aluminum–strontium alloy continuous extrusion under large strain[J]. Rare Metal Materials and Engineering,2023,52(3):1094~1102.]
DOI:10.12442/j. issn.1002-185X.20220165

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  • 收稿日期:2022-03-02
  • 最后修改日期:2022-05-07
  • 錄用日期:2022-05-19
  • 在線發(fā)布日期: 2023-04-07
  • 出版日期: 2023-03-24