2和FeSn2,惰性潤濕界面未析出反應(yīng)產(chǎn)物且存在微孔隙缺陷. 熔池中心處的界面IMCs層厚最大,IMCs層厚約為6 μm,隨著測(cè)試位置逐漸遠(yuǎn)離熔池中心,界面IMCs層厚呈非線性遞減趨勢(shì)。"/>

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鋼/鉛雙金屬結(jié)構(gòu)熔滴沉積復(fù)合TIG電弧增材制造工藝與界面組織研究
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西安交通大學(xué)

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民用航天技術(shù)預(yù)先研究資助(項(xiàng)目號(hào)D020208),江蘇高校省級(jí)重點(diǎn)實(shí)驗(yàn)室開放研究課題資助(項(xiàng)目號(hào)KJS1809)和航空科學(xué)基金資助(項(xiàng)目號(hào)20200054070001)


Investigation on the interfacial microstructure of the steel/lead bimetallic structure fabricated by the hybrid TIG arc and droplet deposition manufacturing
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    摘要:

    采用熔滴沉積復(fù)合鎢極氬弧焊(TIG)電弧增材制造工藝實(shí)現(xiàn)了45鋼/錫鉛合金雙金屬結(jié)構(gòu)的直接冶金結(jié)合. 利用金相顯微鏡、掃描電鏡、X射線衍射等研究了鋼/鉛雙金屬增材制造結(jié)構(gòu)界面不同位置特征區(qū)域的金相組織、界面元素分布和主要物相. 結(jié)果表明,采用熔滴沉積復(fù)合TIG電弧增材制造工藝成形的鋼/鉛雙金屬結(jié)構(gòu)界面無明顯裂紋、孔隙等宏觀冶金缺陷;根據(jù)鋼/鉛界面金屬間化合物(IMCs)的分布狀態(tài)判定,鉛合金熔滴在45鋼表面的沖擊、鋪展過程中,同時(shí)存在“反應(yīng)性潤濕”和“惰性潤濕”,反應(yīng)性潤濕界面存在微小波動(dòng)并且界面處IMCs為FeSb2和FeSn2,惰性潤濕界面未析出反應(yīng)產(chǎn)物且存在微孔隙缺陷. 熔池中心處的界面IMCs層厚最大,IMCs層厚約為6 μm,隨著測(cè)試位置逐漸遠(yuǎn)離熔池中心,界面IMCs層厚呈非線性遞減趨勢(shì)。

    Abstract:

    The direct metallurgical bonding of C45 steel/tin-lead alloy bimetallic structures was achieved by the hybrid TIG arc and droplet deposition manufacturing. The microstructure, interface element distribution and main phases of the steel/lead bimetallic structure were studied by metallurgical microscopy, scanning electron microscopy and X-ray diffraction. The results indicated that the steel/lead bimetallic structure interface formed by the droplet deposition composite TIG arc additive manufacturing process are no obvious cracks, pores and other macroscopic metallurgical defects; According to the distribution of intermetallic compounds (IMCs) at the steel/lead interface, there is both "reactive wetting" and "inert wetting" during the impact and spreading of lead alloy droplets on the C45 steel substrate, where the reactive wetting interface has small fluctuations and the IMCs at the interface are FeSb2 and FeSn2, and the inert wetting interface does not precipitate reaction products and has tiny pore defects. The IMCs layer thickness at the center of the molten pool is the largest, and the IMCs layer thickness is about 6 μm. The IMCs layer thickness at the interface shows a non-linear decreasing trend as the test position gradually moves away from the center of the molten pool.

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張永恒,杜軍,郭鑫鑫.鋼/鉛雙金屬結(jié)構(gòu)熔滴沉積復(fù)合TIG電弧增材制造工藝與界面組織研究[J].稀有金屬材料與工程,2023,52(3):1079~1086.[Zhang Yongheng, Du Jun, Guo Xinxin. Investigation on the interfacial microstructure of the steel/lead bimetallic structure fabricated by the hybrid TIG arc and droplet deposition manufacturing[J]. Rare Metal Materials and Engineering,2023,52(3):1079~1086.]
DOI:10.12442/j. issn.1002-185X.20220160

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  • 收稿日期:2022-03-01
  • 最后修改日期:2022-05-21
  • 錄用日期:2022-06-16
  • 在線發(fā)布日期: 2023-04-07
  • 出版日期: 2023-03-24