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HCP結(jié)構(gòu)TiZrHf中熵合金變形行為的準(zhǔn)原位EBSD研究
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1.西安交通大學(xué);2.金屬材料強(qiáng)度國家重點(diǎn)實(shí)驗(yàn)室

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國家自然科學(xué)基金資助(51801147,51790482)


Quasi-In-Situ EBSD Study On The Deformation Behavior Of TiZrHf Medium Entropy Alloys With HCP Structure
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    摘要:

    使用真空電弧爐熔煉出TiZrHf中熵合金和純Ti,利用冷軋及退火得到再結(jié)晶后的等軸晶粒,并采用 X射線衍射方法研究其相組成;使用掃描電鏡和EBSD對TiZrHf合金和純Ti組織進(jìn)行表征并進(jìn)行滑移跡線分析。結(jié)果表明: TiZrHf合金與純Ti都為單相HCP結(jié)構(gòu)且軸比接近,經(jīng)再結(jié)晶后織構(gòu)類型都為基面織構(gòu)。在室溫下沿RD拉伸變形10%時(shí),TiZrHf合金的錐面滑移開動比例為26%,接近純Ti中錐面滑移晶粒占比的兩倍,且生成{10-12}拉伸孿晶的數(shù)量明顯多于純Ti。

    Abstract:

    : TiZrHf medium entropy alloy and pure Ti were prepared in vacuum arc furnace. The equiaxed grains were obtained by cold rolling and annealing, and their phase composition was studied by X-ray diffraction. Scanning electron microscope and Electron back scattered diffraction was performed to study the microstructure and in-grain slip activities of TiZrHf alloy and pure Ti. The results show that both TiZrHf alloy and pure Ti are single-phase HCP structure with approximately the same axial ratio, and their texture are basal texture after recrystallization. The pyramidal slip of TiZrHf alloy occupy a high fraction of~26% at 10% tensile strain along RD, which is twice the proportion of pyramidal slip in pure Ti, and the number of {10-12} tensile twins is significantly more than that of pure Ti.

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張玉晴,張東東,匡杰,易萌,劉剛,孫軍. HCP結(jié)構(gòu)TiZrHf中熵合金變形行為的準(zhǔn)原位EBSD研究[J].稀有金屬材料與工程,2023,52(2):719~727.[Zhangyuqing, Zhang Dongdong, Kuang Jie, Yi Meng, Liu Gang, Sun Jun. Quasi-In-Situ EBSD Study On The Deformation Behavior Of TiZrHf Medium Entropy Alloys With HCP Structure[J]. Rare Metal Materials and Engineering,2023,52(2):719~727.]
DOI:10.12442/j. issn.1002-185X.20220069

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歷史
  • 收稿日期:2022-01-22
  • 最后修改日期:2022-04-02
  • 錄用日期:2022-04-25
  • 在線發(fā)布日期: 2023-03-09
  • 出版日期: 2023-02-28