2AlNb基合金;板條O相;動態(tài)球化行為;硬化模型"/> 2AlNb基合金進行等溫多向鍛造,采用SEM、XRD、EBSD和硬度測試等定量分析了不同變形道次下合金微觀組織和顯微硬度的變化規(guī)律,揭示了板條O相的動態(tài)球化行為和合金硬化機制。結(jié)果表明:隨變形道次的增加,初始粗大板條O相先后經(jīng)歷了動態(tài)機械破碎和動態(tài)再結(jié)晶兩種細化機制,板條完全球化主要發(fā)生在3道次變形過程中;板條O相的動態(tài)球化過程伴隨著彎曲、扭折、剪切和晶粒撕裂這四種變形行為,后兩類變形的機制可概括為:O/O相界分離、B2相嵌入、O相分離和O相球化;3道次變形后初始板條O相細化至1.3μm的等軸組織,細小等軸O相含量高達68.84%,此時合金硬度較初始樣提高了103.55HV,晶界硬化機制的貢獻占比為64%。"/>

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Ti2AlNb基合金等溫多向鍛造板條O相球化行為和硬化機制研究
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合肥工業(yè)大學 材料科學與工程學院

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國家自然科學基金資助項目(51975175,51875158)


Spheroidization behavior and hardening mechanism of the lath Ti2AlNb-based alloy during multi-directional isothermal forging
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School of Materials Science and Engineering,Hefei University of Technology,Hefei 23009,China

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    摘要:

    在800℃下對Ti2AlNb基合金進行等溫多向鍛造,采用SEM、XRD、EBSD和硬度測試等定量分析了不同變形道次下合金微觀組織和顯微硬度的變化規(guī)律,揭示了板條O相的動態(tài)球化行為和合金硬化機制。結(jié)果表明:隨變形道次的增加,初始粗大板條O相先后經(jīng)歷了動態(tài)機械破碎和動態(tài)再結(jié)晶兩種細化機制,板條完全球化主要發(fā)生在3道次變形過程中;板條O相的動態(tài)球化過程伴隨著彎曲、扭折、剪切和晶粒撕裂這四種變形行為,后兩類變形的機制可概括為:O/O相界分離、B2相嵌入、O相分離和O相球化;3道次變形后初始板條O相細化至1.3μm的等軸組織,細小等軸O相含量高達68.84%,此時合金硬度較初始樣提高了103.55HV,晶界硬化機制的貢獻占比為64%。

    Abstract:

    Multidirectional isothermal forging (MIF) experiments of Ti2AlNb-based alloy was carried at 800°C. The microstructure evolution and hardness of the alloy under different deformation cycles were quantitatively analyzed by SEM, XRD, EBSD and hardness testing. The dynamic spheroidization behavior of the lath O and alloy hardening mechanism was revealed. The results show that as the number of deformation cycles increases, the initial coarse lath O has undergone two refinement mechanisms, namely dynamic mechanical breaking and dynamic recrystallization. The globalization of the lath mainly occurs in 3 cycles deformation process. The dynamic spheroidization process is accompanied by four deformation behaviors: bending, kinking, shearing and grain tearing. The mechanism of the latter two types of deformation can be summarized as: O/O phase boundary separation、penetration of B2 phase、O phase separation and O phase spheroidization. The initial lath O phase is refined to 1.3 μm equiaxed structure, and the percentages of fine equiaxed O phase is as high as 68.84% after 3 cycles of MIF. At this time, the hardness of the alloy is 103.55HV higher than the initial sample, and the contribution of grain boundary hardening mechanism is 64%.

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李 萍,黃曉雨,劉 樂,郭勝華,薛克敏. Ti2AlNb基合金等溫多向鍛造板條O相球化行為和硬化機制研究[J].稀有金屬材料與工程,2023,52(2):685~691.[LI Ping, HUANG Xiao-yu, LIU Le, GUO Sheng-hua, XUE Ke-min. Spheroidization behavior and hardening mechanism of the lath Ti2AlNb-based alloy during multi-directional isothermal forging[J]. Rare Metal Materials and Engineering,2023,52(2):685~691.]
DOI:10.12442/j. issn.1002-185X.20220061

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  • 收稿日期:2022-01-20
  • 最后修改日期:2022-03-18
  • 錄用日期:2022-03-28
  • 在線發(fā)布日期: 2023-03-09
  • 出版日期: 2023-02-28