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直流電弧熱等離子體球化處理TA1粉末工藝研究
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作者單位:

1.黑龍江省科學(xué)院高技術(shù)研究院;2.航天海鷹哈爾濱鈦業(yè)有限公司

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中圖分類號(hào):

TG146.2

基金項(xiàng)目:

黑龍江省“百千萬(wàn)”工程科技重大專項(xiàng)(2020ZX10A03) ;黑龍江省重點(diǎn)研發(fā)計(jì)劃(GA21A104)


Study on the process of TA1 powder spheroidization by DC arc thermal plasma
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Affiliation:

1.Institute of Advanced Technology,Heilongjiang Academy of Sciences;2.Aerospace Haiying Harbin Titanium Co,Ltd

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    摘要:

    采用直流電弧熱等離子體對(duì)不規(guī)則TA1粉末進(jìn)行球化處理。利用金相顯微鏡、掃描電子顯微鏡、粒度粒形分析儀、霍爾流量計(jì)及氧氮分析儀等分析測(cè)試手段,研究球化工藝對(duì)粉末組織形貌、粒度、球形度、流動(dòng)性、松裝密度及氧含量的影響。結(jié)果表明,球化處理可將不規(guī)則形狀TA1粉末球化為表面附著一層納米顆粒的實(shí)心球形;粉末內(nèi)部組織由等軸狀α相轉(zhuǎn)變?yōu)殚L(zhǎng)條狀α相。球化處理使TA1粉末平均粒徑和氧含量降低,球形度升高。原料粉末粒度越小、等離子體發(fā)生器功率越高,球化后粉末平均粒徑越小,球形度越高;但會(huì)導(dǎo)致球化后粉末中納米顆粒含量升高、粉末流動(dòng)性變差、松裝密度降低;去除納米顆??梢蕴岣叻勰┝鲃?dòng)性,進(jìn)一步降低氧含量。

    Abstract:

    In this work, the irregular TA1 powder was spheroidized by DC arc thermal plasma. Metallographic microscope, scanning electron microscope, particle size analyzer, Hall flowmeter and oxygen-nitrogen analyzer were used to study the particle size of raw material powder and the power of plasma generator in the process of spheroidization, and the effects on the microstructure, particle size, sphericity, fluidity, bulk density and oxygen content of the spheroidized powder. The results show that the irregular TA1 powder was spheroidized into solid spherical powder with uniform particle size after thermal plasma spheroidization. The surface was coated with a layer of nanoparticles. After spheroidization, the internal structure of the powder changed from the initial equiaxed α phase to the long strip α phase. The average particle size and oxygen content of TA1 powder decreased and the sphericity increased by thermal plasma spheroidization. The smaller the particle size of raw powder and the greater the power of plasma generator, the smaller the average particle size of spheroidized powder and the higher the sphericity, too small particle size of raw material powder and too high power of plasma generator will lead to the increase of nano-particle content in the powder after spheroidization, the deterioration of powder fluidity and the decrease of bulk density. After removing nanoparticles can improve the fluidity of powder.

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宋美慧,李巖,張煜,李艷春,張曉臣,陳卓,韓芳明.直流電弧熱等離子體球化處理TA1粉末工藝研究[J].稀有金屬材料與工程,2023,52(2):617~622.[Song Meihui, Li Yan, Zhang Yu, Li Yanchun, Zhang Xiaochen, Chen Zhuo, Han Fangming. Study on the process of TA1 powder spheroidization by DC arc thermal plasma[J]. Rare Metal Materials and Engineering,2023,52(2):617~622.]
DOI:10.12442/j. issn.1002-185X.20220038

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歷史
  • 收稿日期:2022-01-15
  • 最后修改日期:2022-02-09
  • 錄用日期:2022-03-07
  • 在線發(fā)布日期: 2023-03-09
  • 出版日期: 2023-02-28