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基于熱加工圖的均勻化態(tài)GH4151合金熱變形行為研究
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北京科技大學(xué) 材料科學(xué)與工程學(xué)院

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高溫結(jié)構(gòu)材料重點(diǎn)實(shí)驗(yàn)開放基金和中央高?;究蒲袠I(yè)務(wù)費(fèi)資助(項(xiàng)目號FRF-TP-19-038A2)


Research on Hot Deformation Behavior of Homogenized GH4151 Alloy Based on Hot Processing Map
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School of Materials Science and Engineering,University of Science and Technology Beijing

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    摘要:

    高性能航空發(fā)動(dòng)機(jī)的發(fā)展亟需可在800℃以上服役的渦輪盤用高溫合金。通過提升γ′相含量,可顯著提升高溫合金熱強(qiáng)性。GH4151合金是高γ′相含量高溫合金的典型代表,在熱力學(xué)平衡態(tài)下γ′相含量約55 wt.%,合金服役溫度高達(dá)800℃,應(yīng)用前景廣闊。然而高含量的γ′相也增大了變形難度。對均勻化后的鑄錠進(jìn)行開坯是高溫合金盤鍛件制備中的重要環(huán)節(jié),但目前關(guān)于均勻化態(tài)GH4151合金熱變形行為的研究仍缺乏系統(tǒng)。因此本文對均勻化態(tài)GH4151合金進(jìn)行等溫?zé)崮M壓縮實(shí)驗(yàn),基于流變曲線構(gòu)建熱加工圖,通過場發(fā)射掃描電子顯微鏡(FESEM),能譜耦合電子背散射衍射(coupled EBSD/EDS)等表征方法觀察分析熱變形組織。基于熱加工圖得到變形安全區(qū)為1060 ~ 1090 ℃,0.1 ~ 0.2 s-1, 及1060 ~ 1070 ℃,0.1 ~1 s-1。初始組織內(nèi)大量存在的一次γ′相(γ′Ⅰ相)阻礙位錯(cuò)運(yùn)動(dòng),促進(jìn)再結(jié)晶,并且釘扎晶界,細(xì)化晶粒。隨著變形量的增加,失穩(wěn)區(qū)逐漸擴(kuò)大。GH4151合金主要失穩(wěn)形式為變形試樣鼓肚處存在的拉應(yīng)力誘導(dǎo)晶界及γ/γ′Ⅰ相界開裂,提高變形溫度及變形速率會(huì)加重開裂。

    Abstract:

    Superalloy that can serve above 800 °C is urgently needed for the development of high-performance aero-engine turbine disk. Increasing the content of γ′ phase could significantly improve high temperature machinal properties, and GH4151 alloy is the typical representative of superalloys with more γ′ phase, and its γ′ phase content is about 55 wt.%. Besides, GH4151 alloy could serve at 800 ℃ and presents a broad application prospect. However, the higher content of γ′ phase also increases the difficulty of deformation. Cogging process of the homogenized ingot is an important part in preparation of turbine discs. However, there is still a lack of systematic research on the hot deformation behavior of homogenized GH4151 alloy. Therefore, the deformation behavior of homogenized GH4151 alloy was studied by isothermal hot compression test and hot processing maps were established based on flow curves. In addition, FESEM and coupled EBSD/EDS methods were utilized to analyze deformed microstructure. Based on the results of hot processing map, the domains with good workability are 1060 ~ 1090 ℃,0.1 ~ 0.2 s-1 and 1060 ~ 1070 ℃,0.1 ~1 s-1. A large amount of primary γ′ phase (γ′Ⅰ) in initial structure hinders the movement of dislocations to promote recrystallization, and pins the grain boundaries to refine the grains. An increasing deformation strain contributes to a larger instability domain. The main form of GH4151 alloy deformation instability is that the tensile stress at the bulging zone of deformed sample induces cracking of grain boundary and γ/γ′Ⅰ phase boundary. Increasing deformation temperature and deformation rate will promote cracking.

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引用本文

王 法,江 河,董建新.基于熱加工圖的均勻化態(tài)GH4151合金熱變形行為研究[J].稀有金屬材料與工程,2023,52(1):245~252.[Wang Fa, Jiang He, Dong Jianxin. Research on Hot Deformation Behavior of Homogenized GH4151 Alloy Based on Hot Processing Map[J]. Rare Metal Materials and Engineering,2023,52(1):245~252.]
DOI:10.12442/j. issn.1002-185X.20211128

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  • 收稿日期:2021-12-18
  • 最后修改日期:2022-01-29
  • 錄用日期:2022-03-07
  • 在線發(fā)布日期: 2023-02-13
  • 出版日期: 2023-02-08