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一種新型鎳基粉末高溫合金組織與性能研究
作者:
作者單位:

1.中南大學(xué) 粉末冶金研究院;2.深圳市萬澤中南研究院有限公司

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基金項目:

廣東省重點領(lǐng)域研發(fā)計劃項目(2019B010935001),國家科技重大專項(2017-VI-0009-0080)和深圳市工業(yè)和信息化局項目(201806071403422960)


The Microstructure and Properties of a novel Nickel-based P/M Superalloy
Author:
Affiliation:

Powder Metallurgy Research Institute of Central South University

Fund Project:

National Science and Technology Major Project(2017-Ⅵ-0009-0080)Industry and Information Technology Bureau of Shenzhen Municipality (Project No. 201806071403422960)

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    摘要:

    利用掃描電子顯微鏡、光學(xué)顯微鏡、疲勞試驗機(jī)、拉伸試驗機(jī)等研究了一種新型鎳基粉末高溫合金(WZ-A3)不同狀態(tài)下的顯微組織、拉伸性能、低周疲勞性能及其斷口形貌。結(jié)果表明:1150℃擠壓消除了合金熱等靜壓殘余的粉末原始顆粒邊界(Previous Particle Boundary,PPB)。隨著溫度提高,熱等靜壓+熱處理(WZ-A3-HIP)和熱等靜壓+熱擠壓+熱處理(WZ-A3-HEX)兩種狀態(tài)樣品拉伸強(qiáng)度呈現(xiàn)出先下降(室溫到400℃)到不變(400~550℃)再下降(550~800℃)的變化規(guī)律。觀察拉伸斷口發(fā)現(xiàn)室溫PPB降低了WZ-A3-HIP樣品延伸率,700℃升高800℃時兩種狀態(tài)樣品斷口由穿晶-沿晶混合型轉(zhuǎn)變?yōu)檠鼐嗔涯J綖橹鳌P?yīng)變(0.6%、0.8%)控制疲勞時,WZ-A3-HEX樣品疲勞壽命值優(yōu)于WZ-A3-HIP,后者裂紋源主要由夾雜物引起。大應(yīng)變(1.0%、1.2%、1.4%)時,兩種狀態(tài)樣品壽命值接近。應(yīng)變1.2%時,疲勞裂紋源均為多源平臺型斷裂。

    Abstract:

    In order to study the microstructure, tensile properties, strain-controlled low cycle fatigue properties and fracture morphology of a novel nickel-based powder metallurgy(P/M) superalloy (WZ-A3) under different conditionss, the scanning electron microscopy, optical metalloscopy, fatigue testing machine and tensile testing machine were used.The results show that the Previous Particle Boundary (PPB) formed during the Hot Isostatic Pressing (HIP) process were fully eliminated by Hot Extrusion (HEX). With the increase of tensile temperature from room temperature to 800℃, the tensile strength of the alloy decreases first (from room temperature to 400℃), remains unchanged (from 400℃ to 550℃), and then decreases (from 550℃ to 800℃). At room temperature, The Elongation of the HIP+HT samples were reduced by PPB. From 700℃ to 800℃, these two states of the tensile fracture changed from the mixed transgranular and intergranular fracture mode to the intergranular fracture mode. The fatigue life (Nf) of HIP+HEX+HT samples was higher than that of HIP +HT samples under small strain control (0.6%, 0.8%), which was related to inclusions in the alloy. When the strain was large (1.0%, 1.2%, 1.4%), the Nf were close to each other. When the strain was 1.2%, the multiple platform-type fatigue crack sources appeared in both samples.

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引用本文

楊金龍,龍安平,張高翔,郭建政.一種新型鎳基粉末高溫合金組織與性能研究[J].稀有金屬材料與工程,2022,51(3):1031~1039.[yangjinlong, Long Anping, Zhang Gaoxiang, Guo Jianzheng. The Microstructure and Properties of a novel Nickel-based P/M Superalloy[J]. Rare Metal Materials and Engineering,2022,51(3):1031~1039.]
DOI:10.12442/j. issn.1002-185X.20210156

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  • 收稿日期:2021-02-26
  • 最后修改日期:2021-06-30
  • 錄用日期:2021-07-09
  • 在線發(fā)布日期: 2022-04-06
  • 出版日期: 2022-03-30