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熱處理對熱電Bi2Te2.7Se0.3“納米花”材料形貌的影響
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作者單位:

1.商洛學(xué)院;2.西安建筑科技大學(xué)環(huán)境與市政工程學(xué)院

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基金項(xiàng)目:

國家自然科學(xué)基金資助(項(xiàng)目號No.21873063)和商洛學(xué)院科研基金資助(項(xiàng)目號:19SKY001)


The Effect of Thermal Treatment on the Morphology of Flower-shaped Thermoelectric Bi2Te2.7Se0.3 Materials
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Affiliation:

1.Shaanxi Key Laboratory of Comprehensive Utilization of Tailings Resources,Shangluo University;2.School of Environment Municipal Engineer,Xi’an University of Architecture and Technology,Xi’an

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    摘要:

    采用bottom-up制備納米材料技術(shù),在ITO導(dǎo)電玻璃上電化學(xué)恒電位沉積制備了一種由納米線變異為納米帶,進(jìn)而構(gòu)成的“納米花”形貌的熱電材料。采用FE-SEM技術(shù)手段對納米花形貌進(jìn)行研究,探討了熱電納米花材料的形成機(jī)理,模擬了納米花形成過程。結(jié)果分析表明,納米花是經(jīng)過兩個(gè)階段形成的:首先是納米線在熱處理過程逐漸形成納米帶,然后,由納米帶收縮形成納米花;熱處理?xiàng)l件對納米花的形成起到?jīng)Q定性的作用。

    Abstract:

    Following the bottom-up technology, the flower-shaped nanomaterials consisted of nanobelts and nanowirs were fabricated on ITO-coated glass substrate by electrodeposition. The morphology of the as-prepared nano-flower was analized by FE-SEM. Moreover, the forming process was simulated. The results showed that the nano-flowers were fabricated through the two steps: first, nanowires formed gradually into nanobelts during the couse of thermal treatment; second, nanobelts contracted into nano-flowers. In addition, the conditions of thermal treatment played the determined role on the flower-shaped Bi2Te2.7Se0.3thermoelectric materials.

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引用本文

李曉龍,周春生,楊超普,李哲建,邸友瑩,李峰,王晴玉,郭明.熱處理對熱電Bi2Te2.7Se0.3“納米花”材料形貌的影響[J].稀有金屬材料與工程,2021,50(11):3966~3970.[Li Xiaolong, Zhou Chunsheng, Yang Chaopu, Li Zhejian, Di Youying, Li Feng, Wang Qingyu, Guo Ming. The Effect of Thermal Treatment on the Morphology of Flower-shaped Thermoelectric Bi2Te2.7Se0.3 Materials[J]. Rare Metal Materials and Engineering,2021,50(11):3966~3970.]
DOI:10.12442/j. issn.1002-185X.20200857

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  • 收稿日期:2020-11-08
  • 最后修改日期:2020-11-28
  • 錄用日期:2020-12-23
  • 在線發(fā)布日期: 2021-11-30
  • 出版日期: 2021-11-24