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薄板試樣定向凝固枝晶競爭生長
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1.中國航發(fā)北京航空材料研究院 先進高溫結(jié)構(gòu)材料重點實驗室;2.東北大學(xué) 軋制技術(shù)及連軋自動化國家重點實驗室;3.鄭州大學(xué) 材料科學(xué)與工程學(xué)院;4.西北工業(yè)大學(xué)凝固技術(shù)國家重點實驗室

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本課題受中國航發(fā)產(chǎn)學(xué)研合作項目HFZL2018CXY022及航材院益材KJ53200134資助


The competitive growth of dendrite arrays in the directional growth of a thin sample
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1.Science and Technology on Advanced High Temperature Structural Materials Laboratory,Beijing Institute of Aeronautical Materials;2.State Key Laboratory of Rolling and Automation,Northeastern University,Shenyang;3.School of Materials Science and Engineering,Zhengzhou University

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    摘要:

    深入理解高溫合金定向凝固雜晶演化具有重要的科學(xué)和工程意義,其中枝晶競爭生長是揭示晶界演化與淘汰的關(guān)鍵環(huán)節(jié)。定向凝固雙晶競爭生長的實驗研究證實了傳統(tǒng)尖端過冷度理論的局限性,定量相場模擬的研究獲得了大量統(tǒng)計規(guī)律,促進了人們對定向凝固雙晶競爭生長的理解。本文在薄板狀試樣的定向凝固過程中,同時獲得了大量的不同取向的枝晶競爭生長,通過拼接金相顯微組織同時獲得多個晶界的取向演化規(guī)律。在多次實驗的基礎(chǔ)上最終獲得實驗統(tǒng)計結(jié)果,與相場模擬結(jié)果基本一致。后續(xù)采用商業(yè)軟件ProCAST的CAFE計算晶粒定向競爭生長晶界演化,統(tǒng)計結(jié)果發(fā)現(xiàn)與實驗結(jié)果存在偏差。本次實驗研究檢驗了薄板狀試樣枝晶競爭生長的統(tǒng)計規(guī)律,對認識高溫合金定向凝固過程中晶界取向的演化具有重要的意義。

    Abstract:

    The high performance blade has been the widely applied to increase the efficiency of the aircraft engine, and its fabrication has been well developed. However, the appearance of misoriented grains always decrease of production yield. Competitive growth of dendrite arrays with different orientation in directional solidification is an important phenomenon for the fabrication of single crystal blade. The question has caught attention for many years. The tip undercooling has been the only criterion for the elimination of unrefereed dendritic grains for a long time and is implanted in commercial software ProCAST to simulate the grain growth. However, the experimental bicrystal growth in directional solidification identified the drawback of the tip undercooling criterion. Quantitative phase field simulations showed more details of the bicrystal competitive growth. The grain boundary evolution has been one of the key indicators for competitive growth. The previous tip undercooling criterion could not predict the grain boundary evolution. The huge phase field simulations reveal the statistic evolution rule of the grain boundary direction. In this paper, we proposed a sheet sample with multiple bycrystals configurations. The microstructures were observed in a stitching picture. The competitive growth and the grain boundary selection of dozens of biocrystals have been summarized within several samples. The statistical results agree with the phase field simulation. However, the CAFE simulation results from the ProCAST can not predict the grain boundary evolution. The method proposed here can be applied to investigate the competitive growth with a high throughput way. The results are helpful to understand the unoriented grains in fabrication of single crystal blade.

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楊澤南,張 朕,郭春文,潘 昊,王 禎,張 強,黃朝暉,王志軍.薄板試樣定向凝固枝晶競爭生長[J].稀有金屬材料與工程,2021,50(4):1247~1253.[Yang Zenan, Zhang Zhen, Guo Chunwen, Pan Hao, Wang Zhen, Zhang Qiang, Huang Chaohui, Wang Zhijun. The competitive growth of dendrite arrays in the directional growth of a thin sample[J]. Rare Metal Materials and Engineering,2021,50(4):1247~1253.]
DOI:10.12442/j. issn.1002-185X.20200810

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  • 收稿日期:2020-10-21
  • 最后修改日期:2020-11-16
  • 錄用日期:2020-12-14
  • 在線發(fā)布日期: 2021-05-08
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