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離心霧化制備SAC305球形粉工藝研究
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1.昆明理工大學(xué)材料科學(xué)與工程學(xué)院;2.云南錫業(yè)錫材有限公司

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云南省重大專項(xiàng)(項(xiàng)目號(hào)2018ZE004)


Production of SAC305 Solder Powder by Rotating Atomization Disk
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    摘要:

    為生產(chǎn)高質(zhì)量的SAC305合金球形粉末,研究了轉(zhuǎn)速、處理量、霧化器形狀、氣氛含氧量等工藝參數(shù)對(duì)旋轉(zhuǎn)離心霧化生產(chǎn)Sn-3.0Ag-0.5Cu粉末性能的影響。結(jié)果表明隨著轉(zhuǎn)速(6000-60000rpm)的提高、進(jìn)料量(30-60kg/h)的降低和霧化器尺寸(30-50mm)的增大,SAC305粉末平均粒徑變小,CFD模擬與實(shí)驗(yàn)有一致的趨勢,實(shí)驗(yàn)修正因子n為1.65,CFD模擬修正因子為2.23。杯形霧化盤相比平面霧化盤生產(chǎn)的粉末平均粒徑降低了8%。SEM照片顯示,隨著霧化室氧含量的降低,粉末球形度提高,霧化室中的含氧量低于400ppm時(shí),粉末表面含氧量低于100 ppm,霧化室與熔體的溫差在230℃時(shí)粉末表面質(zhì)量較好。SAC305粉末粒徑和球形度主要受工藝控制,粉體表面質(zhì)量與冷卻效率和收集技術(shù)有關(guān)。

    Abstract:

    In order to produce high-quality SAC305 alloy spherical powder, we studyed the effects of operating parameters: rotating speed, melt feed rate, shape and size of atomizer, and oxygen content in the atomizer chamber on the performance to produce Sn-3.0Ag-0.5Cu powder by rotary centrifugal atomization. It was evidenced from the experimental results that the median size of the atomized powders became smaller with increasing rotating speed(6000-60000rpm), decreasing melt feed rate(30-60kg/h the ), and use of larger atomizer(30-50mm), the experiment value of n is 1.65,the CFD value of n is 1.65. A cup shaped atomizer was able to give approx. 8% finer powder compared to that from a flat-disk shaped one. SEM micrographs revealed that the oxygen content of the atomization chamber decreased, the powder sphericity factor approached 1. When the oxygen content in the atomization chamber was less than 400 ppm, the oxygen content on the powder surface was less than 100 ppm. The surface quality is the best when the superheat of the atomization chamber and the melt is 230℃, the atomization parameters control the particle size and sphericity of the powder. SAC305 powder particle size and sphericity are mainly controlled by the process, and the powder surface quality is related to the cooling efficiency and collection technology.

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隴贊,白海龍,陳東東,段雪霖,嚴(yán)繼康,*易健宏.離心霧化制備SAC305球形粉工藝研究[J].稀有金屬材料與工程,2021,50(9):3313~3319.[Long Zan, Bai Hailong, Chen Dongdong, Duan Xueling, Yan Jikang, Yi Jianhong. Production of SAC305 Solder Powder by Rotating Atomization Disk[J]. Rare Metal Materials and Engineering,2021,50(9):3313~3319.]
DOI:10.12442/j. issn.1002-185X.20200728

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  • 收稿日期:2020-09-19
  • 最后修改日期:2021-01-20
  • 錄用日期:2021-02-03
  • 在線發(fā)布日期: 2021-09-27
  • 出版日期: 2021-09-24