2}孿晶面形核,并不斷消耗1α相而長(zhǎng)大。TB17鈦合金的時(shí)效特征與其他β型鈦合金相似。TB17鈦合金的時(shí)效響應(yīng)快,顯微硬度隨著時(shí)效溫度升高呈現(xiàn)出先增加后降低的趨勢(shì),在450 ℃時(shí)效處理下硬度達(dá)到最大。"/>

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TB17鈦合金在等溫時(shí)效過(guò)程中的相析出行為
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作者單位:

1.南昌航空大學(xué) 材料科學(xué)與工程學(xué)院,江西 南昌 330063;2.南昌航空大學(xué) 江西省航空材料表面技術(shù)工程研究中心,江西 南昌 330063;3.中國(guó)航發(fā)北京航空材料研究院 先進(jìn)鈦合金航空科技重點(diǎn)實(shí)驗(yàn)室,北京 100095

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國(guó)家自然科學(xué)基金項(xiàng)目


Phase Precipitation Behavior of TB17 Titanium Alloy During Isothermal Aging Process
Author:
Affiliation:

1.School of Materials Science and Engineering, Nanchang Hangkong University, Nanchang 330063, China;2.Jiangxi Provincial Engineering Research Center for Surface Technology of Aeronautical Materials, Nanchang Hangkong University, Nanchang 330063, China;3.Aviation Key Laboratory of Science and Technology on Advanced Titanium Alloys, AECC Beijing Institute of Aeronautical Materials, Beijing 100095, China

Fund Project:

National Natural Science Foundation of China (51764041)

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    摘要:

    采用X射線衍射、掃描電子顯微鏡、透射電子顯微鏡和硬度測(cè)試分析了新型超高強(qiáng)韌鈦合金TB17在等溫時(shí)效過(guò)程中析出相的演變及時(shí)效響應(yīng)。結(jié)果表明:該合金在350 ℃時(shí)主要發(fā)生β→β+ω相變,ω相為細(xì)小的顆粒。在450 ℃下進(jìn)行時(shí)效處理時(shí),α相通過(guò)ω相輔助形核的方式形核長(zhǎng)大。在550和650 ℃時(shí)主要發(fā)生β→β+α相變,α相為片層狀。在該溫度范圍內(nèi)長(zhǎng)時(shí)間進(jìn)行時(shí)效處理的TB17合金存在2種類(lèi)型α相,滿(mǎn)足Burgers關(guān)系的1α相和不滿(mǎn)足Burgers關(guān)系的2α相。其中2α相為孿晶α相,在1α相內(nèi)部{102}孿晶面形核,并不斷消耗1α相而長(zhǎng)大。TB17鈦合金的時(shí)效特征與其他β型鈦合金相似。TB17鈦合金的時(shí)效響應(yīng)快,顯微硬度隨著時(shí)效溫度升高呈現(xiàn)出先增加后降低的趨勢(shì),在450 ℃時(shí)效處理下硬度達(dá)到最大。

    Abstract:

    The precipitation phase evolution and the aging response of TB17 titanium alloy, a new titanium alloy with ultra-high strength and toughness, were studied by X-ray diffraction, scanning electron microscope, transmission electron microscope, and Vickers hardness tests during isothermal aging process. The results show that ββ+ω phase transformation mainly happens at 350 °C, and the precipitated phase ω is the shape of fine granular. After aging treatment at 450 °C, the α phase is nucleated through the assistance nucleation of ω phase. The phase transformation of ββ+α occurs at 550 and 650 °C and the α phase exhibits lamellar structure. However, there are two types of α phase precipitated after aging at 550 and 650 °C for long time: the Burgers α (Type 1α) phase which satisfies the Burgers orientation relationship and the Type 2α phase which does not satisfy the Burgers orientation relationship. The Type 2α phase is a twin crystal phase nucleated on the {102} twin plane inside the Burgers α phase. The aging characteristic of TB17 titanium alloy is similar to that of most β type titanium alloys. The aging response of TB17 titanium alloy is fast. The Vickers hardness of TB17 titanium alloy is increased firstly, reaching the maximum value at 450 °C, and then decreased with increasing the aging temperatures.

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羅軍明,朱鴻昌,朱知壽,徐吉林,李明兵.TB17鈦合金在等溫時(shí)效過(guò)程中的相析出行為[J].稀有金屬材料與工程,2021,50(11):3862~3870.[Luo Junming, Zhu Hongchang, Zhu Zhishou, Xu Jilin, Li Mingbing. Phase Precipitation Behavior of TB17 Titanium Alloy During Isothermal Aging Process[J]. Rare Metal Materials and Engineering,2021,50(11):3862~3870.]
DOI:10.12442/j. issn.1002-185X.20200680

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  • 收稿日期:2020-09-08
  • 最后修改日期:2020-11-02
  • 錄用日期:2020-11-23
  • 在線發(fā)布日期: 2021-11-25
  • 出版日期: 2021-11-24