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Mg-9.5Li-2.56Al-2.58Zn合金組織及室溫變形行為
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西安航空學院材料工程學院

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陜西省自然科學基礎研究計劃資助項目(項目號2019JM-247),大學生創(chuàng)新創(chuàng)業(yè)訓練計劃項目(項目號201911736017)


Microstructure and room temperature deformation behavior of Mg-9.5Li-2.56Al-2.58Zn alloy
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1.School of Materials Engineering,Xi’an Aeronautical University,Xi’an 710077;2.China

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    摘要:

    以Mg-9.5Li-2.56Al-2.58Zn合金為研究對象,研究其組織形貌及相組成。并利用UTM5305電子萬能試驗機對其進行了不同應變速率以及不同變形量的壓縮實驗,獲得真實應力-應變曲線,構建合金的室溫變形本構方程。研究壓縮前后的合金微觀組織和壓縮性能演變規(guī)律。結果表明,Mg-9.5Li-2.56Al-2.58Zn合金包含α-Mg、β-Li、Al12Mg17、AlLi和MgLiAl2五相,β-Li為基體相,α-Mg相呈條狀或塊狀,纖維狀Al12Mg17相位于α-Mg相內部,顆粒狀MgLiAl2相分布在晶界上,晶內相AlLi呈顆粒狀。固溶處理后合金組織中析出相的數量明顯減少,合金強度得到提升。根據Mg-9.5Li-2.56Al-2.58Zn合金真實應力-應變曲線分析了應變速率對流變應力的影響,擠壓態(tài)和固溶態(tài)合金室溫壓縮都存在峰值應力和峰值后的軟化現象,有利于室溫成形;并通過線性回歸的方式獲得不同狀態(tài)下的材料本構方程常數n以及l(fā)nA-(Q/RT)的值,構建了基于Arrhenius模型的本構方程。合金組織隨變形量增加被逐漸壓扁、拉長,AlLi相有所增多。

    Abstract:

    The microstructure and phase composition of Mg-9.5Li-2.56Al-2.58Zn alloy were studied. At the same time, the UTM5305 electronic universal testing machine was used to carry out the compression experiments with different strain rate and different deformation amount, to obtain the true stress-strain curve, and to construct the room temperature deformation constitutive equation of the alloy. The microstructure and mechanical properties of the alloy before and after compression were studied.The results show that Mg-9.5Li-2.56Al-2.58Zn alloy consists of five phases: α-Mg, β-Li, Al12Mg17, AlLi and MgLiAl2. β-Li is the matrix phase, α-Mg phase is strip or block, fibrous Al12Mg17 phase is in the interior of α-Mg phase, granular MgLiAl2 phase is distributed on the grain boundary, and intragranular AlLi phase is granular. After solution treatment, the number of precipitates in the alloy structure decreased obviously, and the strength of the alloy increased. According to the real stress-strain curve of Mg-9.5Li-2.56Al-2.58Zn alloy, the effect of strain rate on the flow stress is analyzed. There are peak stress and softening phenomenon after peak value in the compression of extruded and solid solution alloy at room temperature, which is conducive to room temperature forming. The constitutive equation constants n and LnA-(Q/RT) in different states are obtained by linear regression, and the constitutive equation based on Arrhenius model is constructed. With the increase of deformation, the microstructure of the alloy is gradually flattened and elongated, and the AlLi phase is increased.

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張金龍,路恩皓,朱均,張瑩,姜行,尹晨,張祺銘. Mg-9.5Li-2.56Al-2.58Zn合金組織及室溫變形行為[J].稀有金屬材料與工程,2021,50(4):1359~1364.[Jinlong Zhang, Enhao Lu, Jun Zhu, Ying Zhang, Hang Jiang, Chen Yin, Qiming Zhang. Microstructure and room temperature deformation behavior of Mg-9.5Li-2.56Al-2.58Zn alloy[J]. Rare Metal Materials and Engineering,2021,50(4):1359~1364.]
DOI:10.12442/j. issn.1002-185X.20200356

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  • 收稿日期:2020-05-25
  • 最后修改日期:2020-06-23
  • 錄用日期:2020-07-01
  • 在線發(fā)布日期: 2021-05-08
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