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攪拌摩擦加工Al-Pb表面復(fù)合材料的微結(jié)構(gòu)和織構(gòu)
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常熟理工學(xué)院

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TG146.21

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江蘇省高等學(xué)校自然科學(xué)研究重大項(xiàng)目(項(xiàng)目號(hào)18KJA460001)


Microstructure and texture of Al-Pb surface composites fabricated by friction stir processing
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Changshu Institute of Technology

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    摘要:

    本文使用SEM、EBSD、納米壓痕和顯微硬度等測(cè)試技術(shù)分析了攪拌摩擦加工Al-Pb表面復(fù)合材料的微觀組織、織構(gòu)和硬度分布。結(jié)果表明:使用FSP方法制備Al-Pb表面復(fù)合材料,Pb顆粒受到重力和攪拌作用,主要分布于盆狀攪拌加工區(qū)的底部。塑性金屬對(duì)流形成的洋蔥環(huán)結(jié)構(gòu)中,存在富Pb片層和形變鋁基體片層。富Pb片層內(nèi)的Pb顆粒,起到了良好的細(xì)化晶粒作用。變形鋁基體片層分布有少量直徑約100nm的新生Pb粒。受到細(xì)晶強(qiáng)化作用影響,富Pb顆粒區(qū)的硬度顯著高于形變鋁基體。加工區(qū)底部的SZ-AS區(qū)形成強(qiáng)Cube再結(jié)晶織構(gòu);SZ-RS區(qū)形成Cube織構(gòu)和少量Brass織構(gòu);CSZ區(qū)的Cube織構(gòu)較少,{111}織構(gòu)增強(qiáng);上部的AS區(qū)形成強(qiáng)Goss織構(gòu),RS區(qū)織構(gòu)相對(duì)隨機(jī)。

    Abstract:

    The friction stir processing (FSP) was employed to modify 1060 Al surface composites reinforced with Pb particles. The scanning electron microscopy, electron backscatter diffraction, nanoindentation and hardness tester were applied to investigate the microstructure, texture and hardness of Al-Pb surface composites. The results show that the Pb particles are mainly distributed at the bottom of processing area, which is effected by gravity and agitation. In the onion ring structure formed by plastic metal convection, there are Pb-rich zone and deformed Al matrix zone. The Pb particles in the Pb-rich zone play an importent role in grain refinement. A small amount of the new Pb particles (about 100 nm) are distributed in the deformed aluminum matrix. The hardness of Pb-rich zone are significantly higher than that of deformed aluminum matrix. Furthermore, crystallographic texture analysis by electron backscatter diffraction indicates that there are different types of texture in different zone in the processing area. At the bottom of the processing zone, there is a strong Cube texture on SZ-AS. SZ-RS has Cube texture and a small amount of (110)<233> deformation texture, and CSZ has weak Cube texture and {111} texture. At the top, there is a strong Goss texture on AS, but the texture on RS is relatively random.

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許峰.攪拌摩擦加工Al-Pb表面復(fù)合材料的微結(jié)構(gòu)和織構(gòu)[J].稀有金屬材料與工程,2021,50(3):957~962.[xufeng. Microstructure and texture of Al-Pb surface composites fabricated by friction stir processing[J]. Rare Metal Materials and Engineering,2021,50(3):957~962.]
DOI:10.12442/j. issn.1002-185X.20200282

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  • 收稿日期:2020-04-29
  • 最后修改日期:2020-05-12
  • 錄用日期:2020-05-27
  • 在線發(fā)布日期: 2021-04-02
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