-1時(shí),致密度達(dá)到99.55%以上;其組織存在著明顯的各向異性,垂直于構(gòu)建方向的微觀組織呈“棋盤狀”形貌,晶粒大多數(shù)為等軸晶(長徑比為1.828μm)且得到了細(xì)化(dmean=11.226μm),尤其熔池搭接區(qū)域晶粒更加細(xì)小(5μm以下),而平行于構(gòu)建方向?yàn)椤棒~鱗狀”形貌,大多數(shù)為柱狀晶(長徑比為2.831μm),晶粒直徑較大(dmean=25.964μm)。同時(shí)SLM成形GH3536鎳基高溫合金存在明顯的擇優(yōu)取向,橫截面上晶粒具有較強(qiáng)的取向< 100 >取向,垂直于構(gòu)建方向和平行于構(gòu)建方向均為立方織構(gòu){100}<001>。此外SLM凝固成形中晶粒生長對晶粒內(nèi)晶體取向演變有著顯著影響,縱截面變形晶粒內(nèi)的晶體取向變化不明顯,縱截面變形晶粒內(nèi)的晶體取向變化比較明顯,這是由于SLM成形具有極高的溫度梯度和快速的冷卻速率(105K/s)導(dǎo)致的。"/>

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激光選區(qū)熔化GH3536鎳基高溫合金的微觀組織和晶體取向
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國家自然科學(xué)基金資助(項(xiàng)目號No.51875452;No.51804251)


Microstructure and Crystal Orientation of nickel-based superalloy GH3536 by Selective selective laser melting
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    采用激光選區(qū)熔化方法制備了高致密度GH3536鎳基高溫合金塊狀試件,分析了激光選區(qū)熔化成形GH3536合金顯微組織和晶體取向。結(jié)果表明:隨著激光能量密度的升高,成形試樣的致密度先升高后降低,當(dāng)激光能量密度為180~230J.m-1時(shí),致密度達(dá)到99.55%以上;其組織存在著明顯的各向異性,垂直于構(gòu)建方向的微觀組織呈“棋盤狀”形貌,晶粒大多數(shù)為等軸晶(長徑比為1.828μm)且得到了細(xì)化(dmean=11.226μm),尤其熔池搭接區(qū)域晶粒更加細(xì)小(5μm以下),而平行于構(gòu)建方向?yàn)椤棒~鱗狀”形貌,大多數(shù)為柱狀晶(長徑比為2.831μm),晶粒直徑較大(dmean=25.964μm)。同時(shí)SLM成形GH3536鎳基高溫合金存在明顯的擇優(yōu)取向,橫截面上晶粒具有較強(qiáng)的取向< 100 >取向,垂直于構(gòu)建方向和平行于構(gòu)建方向均為立方織構(gòu){100}<001>。此外SLM凝固成形中晶粒生長對晶粒內(nèi)晶體取向演變有著顯著影響,縱截面變形晶粒內(nèi)的晶體取向變化不明顯,縱截面變形晶粒內(nèi)的晶體取向變化比較明顯,這是由于SLM成形具有極高的溫度梯度和快速的冷卻速率(105K/s)導(dǎo)致的。

    Abstract:

    High density GH3536 ni-based superalloy block specimens were prepared by laser selective melting method, and the microstructure and crystal orientation of GH3536 alloy were analyzed. The results show that with the increase of laser energy density, the density of the formed sampleSincreasedSatSfirstSandSthenSdecreased, When the laser energy density is 180~230J.m-1, the density reaches over 99.55%. The structure has obvious anisotropy, the microstructure perpendicular to the construction direction presented a checkerboard morphology, and most of the grains were equiaxed (the length-diameter ratio was 1.828μm) and were refined (dmean=11.226μm), In particular, the grain size in the lap area of molten pool is finer (less than 5 m). Parallel to the construction direction was the fish scale morphology, most of which were columnar crystals (the length-diameter ratio was 2.831μm), with a larger grain diameter (dmean=25.964μm). Simultaneously, SLM processed GH3536 nickel-based superalloy has obvious preferential orientation. On the cross section, the grain has a strong orientation < 100 > orientation, which is cubic texture {100}<001> perpendicular to and parallel to the construction direction. In addition, grain growth in SLM solidification has a significant effect on the evolution of crystal orientation in grain, the crystal orientation in the deformed grain of the longitudinal section does not change obviously, while the crystal orientation in the deformed grain of the longitudinal section changes obviously, this is due to the extremely high temperature gradient and rapid cooling rate (105K/s) of SLM.

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宗學(xué)文.激光選區(qū)熔化GH3536鎳基高溫合金的微觀組織和晶體取向[J].稀有金屬材料與工程,2020,49(9):3182~3188.[. Microstructure and Crystal Orientation of nickel-based superalloy GH3536 by Selective selective laser melting[J]. Rare Metal Materials and Engineering,2020,49(9):3182~3188.]
DOI:10.12442/j. issn.1002-185X.20200242

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  • 收稿日期:2020-04-12
  • 最后修改日期:2020-05-18
  • 錄用日期:2020-05-19
  • 在線發(fā)布日期: 2020-10-15
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