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冷軋變形量和退火制度對(duì)超快速加熱下5083鋁合金晶粒尺寸的影響
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1.廣西大學(xué) 資源環(huán)境與材料學(xué)院;2.廣西柳州銀海鋁業(yè)股份有限公司

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基金項(xiàng)目:

廣西創(chuàng)新驅(qū)動(dòng)項(xiàng)目(桂科AA17202011-1);廣西自然科學(xué)基金(2018GXNSFAA050048,2017GXNSFAA198271);廣西有色金屬及特色材料加工重點(diǎn)實(shí)驗(yàn)室項(xiàng)目(GXYSSF1809)


Effect of cold rolling deformation and annealing process on grain size of 5083 aluminum alloy under ultra-fast heating
Author:
Affiliation:

1.The college of resources,environment and materials,Guangxi University,Nanning Guangxi;2.Guangxi Liuzhou Yinhai Aluminum Co,Ltd,Guangxi Liuzhou

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the Guangxi Innovation Driving Project (GK AA17202011-1); Guangxi Natural Science Foundation (2018GXNSFAA050048, 2017GXNSFAA198271); Guangxi Key Laboratory Project for Processing Non-ferrous Metals and Characteristic Materials (GXYSSF1809)

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    摘要:

    本文利用Gleeble-3500熱模擬系統(tǒng)和電子背散射衍射(EBSD)技術(shù)對(duì)5083鋁合金的超快速退火組織演變規(guī)律進(jìn)行了研究,探討了快速加熱速度、退火溫度及冷軋變形量對(duì)5083鋁合金晶粒尺寸的影響。5083鋁合金經(jīng)80%的冷軋變形后分別以25 ℃/s、250 ℃/s、500 ℃/s的加熱速度升溫至450 ℃保溫3s后以40 ℃/s冷卻時(shí),平均晶粒尺寸隨加熱速度的增加由7.43 μm細(xì)化至4.98 μm。5083鋁合金經(jīng)80%冷軋變形后在不同退火溫度(350 ℃、400 ℃、420 ℃、450 ℃和500 ℃)下進(jìn)行超快速退火(加熱速度500 ℃/s,保溫時(shí)間3 s,冷卻速度40 ℃/s)后,所得晶粒尺寸先減小再增大,在420 ℃退火時(shí),晶粒尺寸達(dá)到最小為4.82 μm。再結(jié)晶晶粒尺寸受晶界遷移速率和形核率的耦合作用,在350 ℃ ~ 420 ℃超快速退火時(shí),由于快速加熱使形核率急劇增大,而形核溫度較低,使晶界遷移速率較小,導(dǎo)致晶界遷移速率小于形核率,因而再結(jié)晶晶粒尺寸由5.23 μm細(xì)化至4.82 μm;在420 ℃ ~ 500 ℃超快速退火時(shí),形核溫度變高,晶界遷移速率快速增大,則晶界遷移速率大于形核率,使合金晶粒由4.82 μm粗化至6.20 μm,420 ℃是5083鋁合金晶界遷移速率和形核率之間競爭的一個(gè)臨界點(diǎn)。5083鋁合金經(jīng)50%、60%、71.4%、80%和87.5%的冷軋變形后以500 ℃/s的超快速加熱速度升溫至450 ℃保溫3s后以40 ℃/s冷卻,所得平均晶粒尺寸分別為7.94 μm、6.82 μm、6.03 μm、4.98 μm和4.84 μm,隨軋制變形量的增大晶粒尺寸減小,但是冷軋制變量達(dá)到80%以后再進(jìn)行超快速退火晶粒尺寸減小不明顯。

    Abstract:

    GLEEBLE-3500 thermal simulation system and EBSD technology were used to study the microstructure evolution of 5083 aluminum alloy under ultra-fast annealing. The effects of rapid heating rate, annealing temperature and cold rolling deformation on the grain size of 5083 aluminum alloy were discussed. The average grain size of 5083 aluminum alloy was refined from 7.43 μm to 4.98 μm with the increase of the heating rate from 25 ℃/s to 500 ℃/s. After ultra-fast annealing (heating rate 500 ℃ / s, holding time 3 s, cooling rate 40 ℃ / s) at different annealing temperatures (350 ℃, 400 ℃, 420 ℃, 450 ℃ and 500 ℃), the grain size of the 80% cold-rolled 5083 aluminum alloy first decreased and then increased. When annealed at 420 ℃, the minimum grain size was 4.82 μm. The grain size of recrystallization was affected by the interaction of boundary migration rate and nucleation rate. During the ultra-fast annealing at 350 ℃ ~ 420 ℃, the nucleation rate increased sharply due to the rapid heating, while the nucleation temperature was low, which makes the grain boundary migration rate smaller, resulting in the grain boundary migration rate less than the nucleation rate, and the recrystallization grain size was refined from 5.23 μm to 4.82 μm; During the ultra-fast annealing at 420 ℃ ~ 500 ℃, the nucleation temperature became higher and the grain boundary migration rate increased rapidly. The grain boundary migration rate was higher than the nucleation rate, which makes the grain coarsening from 4.82 μm to 6.20 μm. 420 ℃ was a critical point for the competition between the grain boundary migration rate and the nucleation rate of 5083 aluminum alloy. After 50%, 60%, 71.4%, 80% and 87.5% cold rolling, 5083 aluminum alloy was heated to 450 ℃ for 3 s at an ultra-rapid heating rate of 500 ℃ / s and cooled at 40 ℃ / s. The average grain sizes were 7.94 μ m, 6.82 μ m, 6.03 μ m, 4.98 μ m and 4.84 μ m, respectively. With the increase of rolling deformation, the grain size decreased, but after the cold rolling reached 80%, the grain size decreased unobviously.

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引用本文

蘇原明,趙艷君,陳思昊,李留洋,胡治流,王乃賢,覃燕玲.冷軋變形量和退火制度對(duì)超快速加熱下5083鋁合金晶粒尺寸的影響[J].稀有金屬材料與工程,2021,50(3):948~956.[SU YuanMing, ZHAO YanJun, CHEN SiHao, LI LiuYang, HU ZhiLiu, WANG Naixian, QIN Yanling. Effect of cold rolling deformation and annealing process on grain size of 5083 aluminum alloy under ultra-fast heating[J]. Rare Metal Materials and Engineering,2021,50(3):948~956.]
DOI:10.12442/j. issn.1002-185X.20200181

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  • 收稿日期:2020-03-17
  • 最后修改日期:2020-05-19
  • 錄用日期:2020-05-27
  • 在線發(fā)布日期: 2021-04-02
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