mean=37.021μm),晶界較少,晶粒均勻相對穩(wěn)定,當(dāng)α相比例增大時,材料強(qiáng)度減小,塑性升高。同時陶瓷型織構(gòu)強(qiáng)度高,取向明顯,織構(gòu)類型為{11-20}<1-100>,與Y方向呈現(xiàn)約45°的夾角,進(jìn)一步驗證了試樣在(101)、(002)、(101)峰強(qiáng)增加的原因,與織構(gòu)的形成有關(guān);陶瓷型試樣的高溫持久性優(yōu)于石墨型,在溫度(400℃、430℃、460℃)下,持久性應(yīng)力斷裂壽命分別提高了1.174%、15.401、6.998%,均為韌性斷裂,其微觀形貌為韌窩花樣。此外,溫度直接影響TC4鈦合金的持久壽命,隨著溫度升高,TC4鈦合金的應(yīng)力斷裂壽命逐漸降低。"/>

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不同鑄型對TC4鈦合金的微觀組織、織構(gòu)和持久性的影響
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作者單位:

1.西安科技大學(xué)機(jī)械學(xué)院;2.西安交通大學(xué);3.中航光電科技股份有限公司;4.中國船舶重工集團(tuán)公司第七二五研究

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中圖分類號:

TG241;TG249.5

基金項目:

國家自然科學(xué)基金資助(項目號No.51875452;No.51804251);陜西省重點研發(fā)計劃項目(2018YBXM-G-3-2;2017TSCXL-GY-05-01).


Analysis of microstructure, texture and high-temperature durability of TC4 titanium alloy by different molds
Author:
Affiliation:

1.School of Mechanical Engineering,Xi''an University of Science and Technology;2.School of Mechanical Engineering, Xi''an Jiaotong University;3.AVIC Optoelectronic Technology Co., Ltd;4.The 725th Research Institute of China Shipbuilding Industry Corporation

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    摘要:

    研究不同鑄型成型下TC4鈦合金的微觀組織、織構(gòu)和高溫持久性能,利用光學(xué)顯微鏡(OM)、X射線衍射(XRD)、掃描電子顯微鏡(SEM)和電子背散射衍射(EBSD)等觀察和分析TC4鈦合金的顯微組織與持久性斷裂行為。結(jié)果表明:不同鑄型工藝TC4鈦合金的物相均為α相、β相和ω相組成,其中主要物相為α相(90%左右)。與石墨型相比,陶瓷型有利于β→α相變,α相高出5.3%,晶粒平均直徑大(dmean=37.021μm),晶界較少,晶粒均勻相對穩(wěn)定,當(dāng)α相比例增大時,材料強(qiáng)度減小,塑性升高。同時陶瓷型織構(gòu)強(qiáng)度高,取向明顯,織構(gòu)類型為{11-20}<1-100>,與Y方向呈現(xiàn)約45°的夾角,進(jìn)一步驗證了試樣在(101)、(002)、(101)峰強(qiáng)增加的原因,與織構(gòu)的形成有關(guān);陶瓷型試樣的高溫持久性優(yōu)于石墨型,在溫度(400℃、430℃、460℃)下,持久性應(yīng)力斷裂壽命分別提高了1.174%、15.401、6.998%,均為韌性斷裂,其微觀形貌為韌窩花樣。此外,溫度直接影響TC4鈦合金的持久壽命,隨著溫度升高,TC4鈦合金的應(yīng)力斷裂壽命逐漸降低。

    Abstract:

    Investigate the microstructure, texture and high-temperature endurance properties of TC4 titanium alloys under different molds. the optical microscopy (OM), X-ray diffraction (XRD), scanning electron microscopy (SEM), and electron back scattering diffraction (EBSD) were used to observe and analyze the microstructure and persistent fracture behavior of TC4 titanium alloy.The results show that the phases of TC4 titanium alloy by different molds are all composed of α phase, β phase and ω phase, and the main phase is α phase (about 90%). Compared with the graphite type, the ceramic type is favorable for the β→α phase transition, the α phase is 5.3% higher, the average grain size is large (dmean = 37.021μm), the grain boundaries are less, and the grains are relatively uniform and relatively stable. When it is large, the material strength decreases and the plasticity increases. Simultaneously, the ceramic-type texture has high strength and obvious orientation. The texture type is {11-20} <1-100>, and the angle with the Y direction is about 45°, it further verified that the samples are in (101), (002),(101) .The reason for the increase in peak intensity is related to the formation of texture,The high temperature durability of ceramic samples is better than that of graphite. At the temperature (400℃,430℃,460℃), the persistent stress fracture life has increased by 1.174%, 15.401, 6.998%, all of which are ductile fracture. Appearance is a dimple pattern. In addition, temperature directly affects the long-term life of TC4 titanium alloy. as the temperature increases, the stress fracture life of TC4 titanium alloy gradually decreases.

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劉文杰,宗學(xué)文,陳楨,楊雨蒙,楊學(xué)東,盧秉恒.不同鑄型對TC4鈦合金的微觀組織、織構(gòu)和持久性的影響[J].稀有金屬材料與工程,2020,49(8):2880~2887.[liuwenjie, zongxuewen, chenzhen, yangyumeng, yangxuedong, lubingheng. Analysis of microstructure, texture and high-temperature durability of TC4 titanium alloy by different molds[J]. Rare Metal Materials and Engineering,2020,49(8):2880~2887.]
DOI:10.12442/j. issn.1002-185X.20200120

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  • 收稿日期:2020-02-24
  • 最后修改日期:2020-04-05
  • 錄用日期:2020-04-10
  • 在線發(fā)布日期: 2020-09-27
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