高斯織構(gòu)為主,同時(shí)存在部分{111}<112>銅型織構(gòu);材料顯微硬度值大幅提升,由初始28.94 HV提高到56.53 HV,增幅高達(dá)95.33%,且分布均勻性良好。"/>

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等通道球形轉(zhuǎn)角擠壓過程中工業(yè)純鋁的微觀組織演變與力學(xué)性能
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作者單位:

1.徐州工程學(xué)院;2.江蘇徐州工程機(jī)械研究院

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中圖分類號(hào):

TG376

基金項(xiàng)目:

國家自然科學(xué)基金資助(51905462);江蘇省“六大人才高峰”高層次人才選拔培養(yǎng)資助項(xiàng)目(GDZB-127);江蘇省科協(xié)青年科技人才“托舉工程”資助培養(yǎng)項(xiàng)目(蘇科協(xié)發(fā)〔2018〕202號(hào))


Microstructure Evolution and Mechanical Properties of Commercially Pure Aluminum during the process of Equal Channel Angular Extrusion with Spherical Cavity(ECAE-SC)
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Xuzhou University of Technology,Xuzhou

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    摘要:

    突破傳統(tǒng)ECAP變形全過程通道等截面思路,提出一種耦合剪切應(yīng)變和正應(yīng)變于一體的新型等通道球形轉(zhuǎn)角擠壓(Equal channel angular extrusion with spherical cavity,ECAE-SC)工藝。在自行研制的模具上對(duì)工業(yè)純鋁進(jìn)行室溫單道次ECAE-SC擠壓實(shí)驗(yàn),采用OM、EBSD和TEM等技術(shù)手段,研究了ECAE-SC變形過程中工業(yè)純鋁微觀組織的演變規(guī)律,并測試了變形后試樣的顯微硬度。結(jié)果表明,在ECAE-SC工藝劇烈簡單剪切變形誘導(dǎo)下,工業(yè)純鋁僅需1道次擠壓變形即可獲得等軸、細(xì)小、均勻的超細(xì)晶組織,平均晶粒尺寸約為400 nm;工業(yè)純鋁室溫ECAE-SC變形以位錯(cuò)滑移為主并伴有不完全連續(xù)動(dòng)態(tài)再結(jié)晶,其微觀組織經(jīng)歷了剪切帶→位錯(cuò)胞→小角度亞晶→大角度等軸晶粒這一動(dòng)態(tài)演化過程。1道次ECAE-SC變形后,工業(yè)純鋁組織以{110}<001>高斯織構(gòu)為主,同時(shí)存在部分{111}<112>銅型織構(gòu);材料顯微硬度值大幅提升,由初始28.94 HV提高到56.53 HV,增幅高達(dá)95.33%,且分布均勻性良好。

    Abstract:

    A new process named equal channel angular extrusion with spherical cavity (ECAE-SC) is proposed based on the idea of breaking through the equal channel during the whole process of traditional ECAP, which combines positive strain with shear strain. On the self-designed ECAE-SC die, the continuous, efficient and compound severe plastic deformation of commercially pure aluminum was realized in a single pass of ECAE-SC at room temperature. Microstructure evolution of commercially pure aluminum during ECAE-SC process was observed and analyzed by optical microscopy (OM), EBSD and TEM. Moreover, microhardness of the processed materials at different deformation regions was tested. The results show that under the severe plastic deformation induced by simple shear, the equiaxed ultrafine grains with average grain size of 400 nm can be obtained by only one pass of ECAE-SC. The deformation mechanism of ECAE-SC at room temperature is dominated by dislocation slip accompanied with incomplete continuous dynamic recrystallization, and the grain refinement process mainly includes the generation of shear bands, the formation of cellular substructures, the appearance of subgrains with low angle boundaries (LABs) and the formation of equiaxed ultrafine grains with large angle boundaries (HABs). After one pass of ECAE-SC, the main texture of commercially pure aluminum is Gauss texture {110} < 001 >, while some {111} < 112 > copper texture exists. The microhardness of the processed materials on the cross section increases significantly, and the average value increases from 28.94 HV to 56.53 HV, with an increase of 95.33%. Meanwhile, a more uniform hardness distribution is obtained.

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王曉溪,張 翔,莊 翌,陸佳鑫,井新宇.等通道球形轉(zhuǎn)角擠壓過程中工業(yè)純鋁的微觀組織演變與力學(xué)性能[J].稀有金屬材料與工程,2020,49(6):1963~1969.[WANG Xiaoxi, ZHANG Xiang, ZHUANG Yi, LU Jiaxin, JING Xinyu. Microstructure Evolution and Mechanical Properties of Commercially Pure Aluminum during the process of Equal Channel Angular Extrusion with Spherical Cavity(ECAE-SC)[J]. Rare Metal Materials and Engineering,2020,49(6):1963~1969.]
DOI:10.12442/j. issn.1002-185X.20190776

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  • 收稿日期:2019-09-19
  • 最后修改日期:2019-10-21
  • 錄用日期:2019-10-22
  • 在線發(fā)布日期: 2020-07-09
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