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激光選區(qū)熔化成形Kanthal涂層及其微波衰減特性研究
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中科院電子所

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國家自然科學(xué)基金項目(面上項目,重點項目,重大項目)61771454


Microstructure and Microwave Attenuation Properties of Kanthal Coating Prepared by Selective Laser Melting
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    摘要:

    采用兩種球形Kanthal合金粉末(顆粒直徑45-60um和50-70um),通過激光選區(qū)熔化(Selective laser melting, SLM)技術(shù)制備Kanthal涂層。利用光學(xué)顯微鏡、掃描電子顯微鏡(SEM)、X射線衍射儀(XRD)和諧振腔特性測量系統(tǒng)對Kanthal粉末及涂層的表面形貌、顯微組織、相結(jié)構(gòu)和諧振腔品質(zhì)因子進行檢測分析。研究結(jié)果表明:SLM成形Kanthal涂層具有表面粗糙、多孔結(jié)構(gòu)、扁平化的特點,與無氧銅基金屬結(jié)合牢固,形成了冶金結(jié)合界面。其中45-60um球形合金粉末SLM成形涂層加載諧振腔品質(zhì)因子(Quality factor)Q值整體比50-70um粉末成形涂層的Q值低,在頻率2985MHz下微波衰減特性更強。涂層成形過程中形成的Al2O3膜和微孔洞使得合金涂層能夠散射微波,減少了對微波的反射。涂層厚度對微波有干涉損耗,厚度0.55mm的Kanthal涂層加載諧振腔Q值最小,達到2280。Kanthal涂層是以磁衰減為主的復(fù)合衰減材料。

    Abstract:

    Kanthal coatings were fabricated by selective laser melting(SLM) with two kinds of powder, 45-60um and 50-70um in diameter. The coatings surface morphology, microstructure, element distribution, phase structure, and microwave attenuation properties were studied by optical microscope, scanning electron microscopy, X-ray diffraction, and cavity characteristic measurement system. The results indicate that Kanthal coatings have the characteristic of rough surface, porous and flaky structure. The quality factor Q of cavity loaded with coatings fabricated by 45-60um Kanthal sphere powder is lower than that of coatings by 50-70?m Kanthal sphere powder, showing better microwave attenuation properties under the frequency of 2985MHz. Al2O3 thin film and micro void generated in the structure of coatings have the effect of scattering microwave and thus reduce microwave reflection. It is also shown that flattened shape of Kanthal coatings is a good way to suppress eddy currents in high-frequeny electromagnetic field and lead to the formation of easy magnetization planes, which is helpful to enhance the microwave attenuation property. The coating thickness has profound effects on interference loss of microwave. Cavity Q with coating thickness of 0.55mm reached the minimum value of 2280. Kanthal coating is composite material and the main mechanism is attributed to magnetic loss.

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王博鋒.激光選區(qū)熔化成形Kanthal涂層及其微波衰減特性研究[J].稀有金屬材料與工程,2020,49(9):3143~3152.[wang. Microstructure and Microwave Attenuation Properties of Kanthal Coating Prepared by Selective Laser Melting[J]. Rare Metal Materials and Engineering,2020,49(9):3143~3152.]
DOI:10.12442/j. issn.1002-185X.20190669

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  • 收稿日期:2019-08-15
  • 最后修改日期:2019-08-27
  • 錄用日期:2019-09-06
  • 在線發(fā)布日期: 2020-10-15
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