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閉孔CNTs/Al復合泡沫攪拌摩擦焊工藝研究
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1.武漢科技大學;2.武漢理工大學

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基金項目:

國家自然科學基金(51775397);中國汽車產(chǎn)業(yè)創(chuàng)新發(fā)展聯(lián)合基金(U1564202);新能源汽車科學與關鍵技術(shù)學科創(chuàng)新引智基地資助(B17034);湖北省高等學校優(yōu)秀中青年科技創(chuàng)新團隊計劃項目(T201629)


Study on friction stir welding process of closed-cell CNTs/Al composite foam
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Affiliation:

1.Key Laboratory of Metallurgical Equipment and Control Technology of Ministry of Education,Wuhan University of Science and Technology,Wuhan;2.Hubei Key Laboratory of Advanced Technology of Automobile components,Wuhan University of Technology,Wuhan

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    摘要:

    閉孔Al復合泡沫作為一種典型輕質(zhì)高強材料,在汽車及航空航天領域具有明確需求牽引和應用前景。采用傳統(tǒng)方法制備泡沫鋁時,生產(chǎn)工藝復雜、樣品尺寸受限,嚴重阻礙了大規(guī)模生產(chǎn)。本文提出基于攪拌摩擦焊制備閉孔CNTs/Al復合泡沫新工藝,解決制備大面積閉孔復合泡沫的難題。利用掃描電鏡對不同焊接旋轉(zhuǎn)速度的閉孔CNTs/Al復合泡沫預制體及復合泡沫的微觀組織進行分析;采用紅外線測溫儀對焊接過程中預制體溫度分布進行研究。利用電子萬能試驗機對純Al泡沫和不同孔隙率閉孔泡沫的屈服應力和平臺應力進行對比。研究結(jié)果表明:當攪拌頭旋轉(zhuǎn)速度為1000rpm時,閉孔CNTs/Al復合泡沫預制體表面平滑而致密。同時,增強體CNTs均勻分布在復合泡沫預制體橫截面上。在發(fā)泡溫度650℃,680℃和700℃對比可知,最佳發(fā)泡溫度為680℃發(fā)泡15min,泡孔結(jié)構(gòu)均勻,孔隙趨于圓形,最大泡孔直徑為0.48mm。常溫壓縮時,閉孔復合泡沫的應力-應變曲線表現(xiàn)出脆性與韌性相結(jié)合的變形特征??紫堵蕿?0.5%時,閉孔泡沫的屈服應力和平臺應力值最大。同時,與純Al泡沫相比,閉孔泡沫的屈服應力提高了2-2.8倍;平臺應力提高了1.4-2.9倍。

    Abstract:

    Closed-cell Al composite foam with high specific strength and high specific stiffness is a typical lightweight material, which has broad application prospectsSin the fields of automobile and aerospaceSapplication. However, the pore structure of aluminum foams prepared by traditional methods is difficult to control, which seriously hinders the production. In this paper, a new preparation process for closed-cell CNTs/Al composite foam based on friction stir welding was proposed. The microstructure and elemental composition of the CNTs/Al composite foams with different rotationSspeeds (1000-1300rpm) were analyzed by scanning electron microscopy and energy dispersive analysis (SEM/EDS). The temperature distribution of the CNTs/Al precursor foam was studied by infrared thermometer and numerical simulation. The mechanical properties of pure Al foam and the CNTs/Al composite foam with different porosity were compared and analyzed by the quasi-static compression test. The results show that when the rotary speed of the stirring is 1000rpm, the surface of the CNTs/Al precursor foam is smooth and dense. Simultaneously, a blowing agent TiH2, a stabilization agent Al2O3 and reinforcedSphase CNTs are uniformly distributed on the cross section of the composite foam. The comparison between the foaming temperature of 680℃ and 700℃ shows that when the foaming temperature is 680℃ for 15min, the pore structure is uniform and mainly consists of circular pores. TheSmaximum pore diameterSisS0.48mm. Infrared thermometer and numerical simulation temperature field show that the temperature gradually decreases with the increase of the distance to the center of the stirring head, and the peak welding temperature is located in the stirring head which exhibits aSbowl-shaped distribution. The stress-strain curves of the CNTs/Al composite foam show the deformation characteristics combining brittleness and ductility at room temperature. When the porosity is 30.5%, the yield stress and platform stress values of the CNTs/Al composite foam are the largest. Compared with the pure Al foam, the yield stress of the CNTs/Al composite foam is increased by about 2-2.8 times, and the platform stress is increased by about 1.4-2.9 times.

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龐秋,于海洋,胡志力.閉孔CNTs/Al復合泡沫攪拌摩擦焊工藝研究[J].稀有金屬材料與工程,2020,49(8):2845~2854.[Pang Qiu, Yu Haiyang, Hu Zhili. Study on friction stir welding process of closed-cell CNTs/Al composite foam[J]. Rare Metal Materials and Engineering,2020,49(8):2845~2854.]
DOI:10.12442/j. issn.1002-185X.20190664

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  • 收稿日期:2019-08-14
  • 最后修改日期:2019-12-10
  • 錄用日期:2019-12-11
  • 在線發(fā)布日期: 2020-09-27
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