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電極感應(yīng)熔化氬氣霧化中液滴尺寸影響因數(shù)及粉末特性的研究
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作者單位:

1.北京科技大學(xué)材料科學(xué)與工程學(xué)院粉末冶金與先進(jìn)陶瓷研究所 北京 1000008;2.北京科技大學(xué)材料科學(xué)與工程學(xué)院粉末冶金與先進(jìn)陶瓷研究所 北京 100083

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中圖分類號(hào):

TG 132.3+2

基金項(xiàng)目:

中央高校科研基金 FRF-TP-17-044A1


Study on Powder Characteristics and Droplet Size Influence Factor in Electrode Induction Melting Argon Atomization
Author:
Affiliation:

1.university of science and technology beijing;2.university of science and technology Beijing

Fund Project:

the Scientific Research Fund of Central Colleges and Universities(FRF-TP-17-044A1)

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    摘要:

    本文對(duì)電極感應(yīng)熔化氣霧化(Electrode induction melting gas atomization,縮寫EIGA)工藝制備的鎳基高溫合金粉末的物理特性,凝固組織以及內(nèi)部元素分布進(jìn)行研究分析;理論分析了EIGA制粉一次霧化過程中液滴尺寸的影響因數(shù);根據(jù)對(duì)流換熱原理計(jì)算了該工藝中不同尺寸粉末的冷卻速率。結(jié)果表明:EIGA粉末以近球形為主,霍爾流速為(13.4s/50g),D90=121.5μm。粉末表面和內(nèi)部凝固組織顯示,隨著粉末尺寸的增大組織均由微晶向胞狀晶和樹枝晶轉(zhuǎn)變。同時(shí)顆粒表面組織之間的間隙不斷加深,粉末光滑度下降。在霧化氣壓為4MPa條件下時(shí),粉末尺寸與冷卻速率的關(guān)系為:。粉末內(nèi)部沒有明顯的成分偏析現(xiàn)象,但晶軸和晶間的元素分布略有差別。晶軸上Ni、Al、Co、C元素含量較晶間高,晶間的Ti、Mo、Cr、Nb元素含量更高。

    Abstract:

    Abstract: In this paper, we investigated the physical characteristics, solidification microstructure, and inter element distribution of Ni-based superalloy powders, which prepared by electrode induction melting gas atomization (EIGA) process. Some factors on metal droplet size during primary atomization were also deeply analyzed. The cooling rate of different size powders were calculated through convective heat transfer principle. It is found that the EIGA powders are mainly spherical, the Hall flow rate is 13.4s/50g, and the D90 is 121.5μm. The microstructure of powders on surface and internal changes from microcrystals to cell crystals and dendrites increasing with the powder size. At the same time, the smoothness of powders decreases as the gap increases on the surface. The relationship between cooling rate and particle size is |〖dT〗_d/dt|=〖8.98*10〗^(-5)/d^2 , when the atomization gas pressure is 4MPa. There is slightly segregation in crystal axis and intercrystal of powders. The content of Ni, Al, Co, and C in crystal is higher than intergranular, while the content of Ti, Mo, Cr, and Nb in intergranular is much higher.

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楊樂彪,任曉娜,夏敏,孫海濤,呂曉安,葛昌純.電極感應(yīng)熔化氬氣霧化中液滴尺寸影響因數(shù)及粉末特性的研究[J].稀有金屬材料與工程,2020,49(6):2017~2023.[yangLeBiao, RenXiaoNa, xiaMin, SunHaiTao, LvXiaoAn, Ge Changchun. Study on Powder Characteristics and Droplet Size Influence Factor in Electrode Induction Melting Argon Atomization[J]. Rare Metal Materials and Engineering,2020,49(6):2017~2023.]
DOI:10.12442/j. issn.1002-185X.20190401

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  • 收稿日期:2019-05-10
  • 最后修改日期:2019-09-30
  • 錄用日期:2019-10-11
  • 在線發(fā)布日期: 2020-07-09
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