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熱變形對(duì)GH4169合金中NbC析出相尺寸形貌影響研究
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作者單位:

1.貴州大學(xué)材料與冶金學(xué)院;2.貴州安大航空鍛造有限責(zé)任公司

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國(guó)家自然科學(xué)基金資助(項(xiàng)目號(hào)51761003)


Effect of Thermal Deformation on Size and Morphology of NbC Precipitates in GH4169 Alloy
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1.School of Materials and Metallurgy,Guizhou University;2.Guizhou Anda Aviation Forging Co., Ltd

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    摘要:

    通過(guò)Gleeble3500熱模擬試驗(yàn)機(jī)進(jìn)行熱壓縮試驗(yàn)并結(jié)合微觀組織觀察和統(tǒng)計(jì)分析,研究了熱變形對(duì)GH4169合金中NbC顆粒尺寸形貌、分布特征的影響規(guī)律。研究表明壓縮過(guò)程中的絕熱效應(yīng)會(huì)導(dǎo)致試樣心部溫度的進(jìn)一步升高,從而為變形過(guò)程中的NbC回溶提供條件。NbC顆粒與基體在變形過(guò)程中形成的高位錯(cuò)密度區(qū)促進(jìn)了元素的擴(kuò)散,并加速了小曲率半徑的尖角區(qū)域回溶和鈍化。隨變形量的增加NbC回溶趨勢(shì)增加,其平均尺寸與體積分?jǐn)?shù)均呈降低趨勢(shì)。變形過(guò)程金屬流動(dòng)會(huì)促進(jìn)NbC顆粒的位移,在70%的變形量下,NbC顆粒平均間距增加趨勢(shì)顯著高于30%和50%變形量試樣。因此隨變形量的增加,NbC顆粒有從鏈狀→鏈條彎曲→鏈條方向改變→彌散分布的分布特征,促進(jìn)基體中原鏈狀NbC呈細(xì)小、彌散分布。研究結(jié)果為GH4169閃光焊接性能的提高提供了直接的參考。

    Abstract:

    The thermal compression test was carried out by Gleeble 3500 thermal simulator and combined with microstructure observation and statistical analysis to study the effect of thermal deformation on the size and distribution characteristics of NbC particles in GH4169 alloy. Studies have shown that the adiabatic effect during compression leads to a further increase in the core temperature of the sample, thus providing conditions for NbC re-dissolution during the deformation process. The high dislocation density region formed by the NbC particles and the matrix during the deformation process promotes the diffusion of the elements and accelerates the remelting and passivation of the sharp corner regions with small radii of curvature. With the increase of deformation, the NbC remelting tendency increased, and the average size and volume fraction showed a decreasing trend. During the deformation process, the metal flow promotes the displacement of the NbC particles. Under the 70% deformation amount, the average spacing of the NbC particles increases significantly higher than the 30% and 50% deformation samples. Therefore, with the increase of deformation, the NbC particles have a distribution characteristic from chain→chain bending→chain direction→dispersion distribution, which promotes the fine and diffuse distribution of the original chain NbC in the matrix. The results provide a direct reference for the improvement of GH4169 flash soldering performance.

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引用本文

李陽(yáng),魏志堅(jiān),徐平偉,梁益龍,梁宇.熱變形對(duì)GH4169合金中NbC析出相尺寸形貌影響研究[J].稀有金屬材料與工程,2020,49(5):1773~1780.[Yang Li, Zhi-jian Wei, Ping-wei Xu, Yi-long Liang, Yu Liang. Effect of Thermal Deformation on Size and Morphology of NbC Precipitates in GH4169 Alloy[J]. Rare Metal Materials and Engineering,2020,49(5):1773~1780.]
DOI:10.12442/j. issn.1002-185X.20190251

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  • 收稿日期:2019-03-26
  • 最后修改日期:2019-05-21
  • 錄用日期:2019-06-05
  • 在線發(fā)布日期: 2020-06-05
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